GCMS quantitation results for sample AE04028, March 2002

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o ’ Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\MAR2202\4028.D Vial: 34 Acq On : 24 Mar 2002 2:39 am Operator: Sample : gc/ms scan 2/25 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Propanol, 1-(2-methoxypropox Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

12.19 0.53 ug/1 61683 1,4-Dichlorobenzene-d4 12.26

Hit# of 5 Tentative ID MW MolForm CAS# Qual / 1 2 -Propanol,-(2-methoxypropoxy)- 148 C7H16O3 013429-07-7 2 Propane, 1/2-dimethoxy- 104 C5H12O2 007778-85-0 39 3 1-Propane/, 2-(2-hydroxypropoxy)- 134 C6H14O3 000106-62-7 38 4 Hydrazine, 1-methyl-1-propyl- 88C4H12N2 004986-49-6 38 Abundance............ 7 ......... ”............ Scan 778 (12.191 min): 4028.D (-) : m/z 59.0^5 100.00% 59 |

5000-

45 A/ 11.80 12.00 12.20 12.40 12.60

m/z--> —10. 201... 30 394011.. 50 — 60 70 7389 80 -T-f-t-T-rT-p-r-r-r-p-r-r-r-pV-t-r-r-p-r-rT-^^ 90 100 110 120 130 m/ z 45.0.5 14.95% Abundance #9233: 2-Propanol, 1-(2-methoxypropoxy)- 59

5000 1 1 i ■ ■ 1 ■ i ■ ■ 11.80 12.00 12.20 12.40 12.60 31 45 m/ z 43.05 11.05% I In । 73 104 m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance 3" 59 MlLAAen 11.80 12.00 12.20 12.40 12.60 5000 m/ z 41.05 9.68% 31 45 15 39 73 ‘ 11/72,1 1′113111111118 , ।.,,, ।, TTmnr 111 j i, 1 • | 104 ' ! ' ' | ) I I I | I I > | | |

m/z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #6086: 1-Propanol, 2-(2-hydroxypropoxyj- 59 —.. AAA— 11.80 12.00 12.20 12.40 12.60 m/ z 73.10 9.67%

NN M 5000 31 45 103

— - TTTTH+. 75 89 m/z-> 10 20 30 40 50 (60 70 80 90 100 110 120 130 11.80 12.00 12.20...12.40 12.60

4028.D GCMS0308.M Tue Mar 26 10:41:57 2002 Page 2

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