GCMS calibration table data, May 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C: \HPCHEM\ 1 \DATA\MAYO 302\9579.D vial: 9 Acq On 3 May 2002 9:52 pm Operator: Sample GC/MS SCAN 4/24 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 11 9,12-Octadecadienoic acid (Z,Z Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. 29.48 4.85 ug/1 379849 Phenanthrene-dl0 25.58 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 9,12-Octadecadienoic acid (Z,Z)- 280 C18H3202 000060-33-3(95) 2 Oxacyclotetradecane-2,11-dione, 13- 240 C14H24O3 074685-36-2 52 3 cis-9,10-Epoxyoctadecan-l-ol 284 C18H3602 013980-12-6 49 4 Oleic Acid 282 C18H3402 000112-80-1 49 Abundance Scan 2667 (29.481 min): 9579.D (-) m/z 55.05 100.00% 4.1 55 67 81 5000

Al 95 TBT iI 110 4 29 29.20 29.40 29.60 29.80 L al, 23 138 165.... ‘i T“f | i T I । "II I r~f i-1-j- i i-i-i | i"i I T-] r r i i [ i । I I | i I i i 264 280 । f i i I | i r m/z 41.05 94.98% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39476: 9,12-Octadecadienoic acid (Z,Z)- 67 55 81

5000 95 ■ ■ i ■ ■

29.20 29.40 29.60 29.80 109 m/z 67.05 68.07%

’’11111/11/1 11 123 ............................................. 280 Il । । 'i । T । । । । । । । t । । । । । । > i II i" r । '| i i i i ।■ r i i i |“ । ■ j “i “I | i—r

m/z->______ 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #31978: Oxacyclotetradecane-2,11-dione, 13-methyl- 55

29.20 29.40 29.60 29.80 5000 m/z 43.05 62.99% 83 42 68 96 / ! 110 — li II, 222 240 1 1 । 1 1 TIt । I j i । । < । । । । । । । । i y i । ! < । । > । । । । । i i ।। i i i । i i 1I* i i ■ r i—।—T m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 P CAA Abundance #40197: cis-9,10-Epoxyoctadecan-1 -ol TLT 29.20 29.40 29.60 29.80

A m/ Z 69.05 62.57% 67 5000 81

95

TFT T-T-pt , , ,123 , , r ।.... 1 । i , .... , , । 155 171............................. . Ttmmr | , , , । | , , , , | , , , , | , i , , । । । । , । । > A MM ) A InnnFIIIIIttIi m/z-> 40 60 80I 100 120 140 160 180 200 220 240 260 280 29.20 29.40 29.60 29.80

9579 .D GCMS0501.M Mon May 06 10:49:58 2002 Page 11

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