GCMS analysis results for sample AE10610, May 10 2002

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Laboratory report detailing GC/MS analysis of sample AE10610 including surrogate recovery data in May 2002.

NYC-WTC_000045662–000045681

Folder label: “GCMS X 5/3/02 A 5/7/02”

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\MSDCHEM\l\DATA\050702\10610.D Vial : 13 Acq On 7 May 2002 10 : 55 pm Operator: Mclean Sample 5/3 kb Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\l\METHQDS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 10 .psi.,.psi.-Carotene, 7,7', Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

34.00 0.30 ug/L 263133 Perylene-dl2 34.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 .psi.,.psi.-Carotene, 7,7',8,8', . . 547 C40H66 000502-62-5 78 2 Docosa-2,6,10,14,18-pentaen-22-a.. 384 C27H440 1000163-04-7 7 8 3 Squalene 410 C30H50 007683-64-9/ 78 4 4,9,13,17-Tetramethyl-4,8,12,16-.. 316 C22H360 056882-09 Z 72 Abundance Scan 5262 (33.997 min): 10610.D (-5249) (-) m/z 69.10 10 . 00% 69

5000 41 95 136 33.60 33.80 34.00 34.20 34.40 ,t 14)209281............................. ItT ■ 1 I 1 1 1 ■ I 1 - 1 ' I ’ 1 1 1 I ’ ' 1 ‘ I ’ 1 1 ’ I ‘ 1 1 1 I 1 ' - ■ I ■ ' ‘ 1 I 1 1 1 1 I 1 1 1 ‘ I 1 m/ z 81.10 49.90% m/z--> 0 50 100 150 200 250 300 350 400 450 500 550 Abundance #114270: .psi.,.psi.-Carotene, 7,7,,8,8',11,11 ',12,12’,15,... 69

5000 ...............I AAA............... I I I I I I I I I I I III I I I I I I I I I

33.60 33.80 34.00 34.20 34.40

41 95 137 m/ z 41.10 30.05% 341367 409435 477503 546 15 I 177 a —44 111:163191217 245 273299 I | r r i ’( J I i i T | ' । T C । I iii ) i i i s kI i r | 1 । i > । r i ‘i । । । । । । । r

m/z-> 0 50 100 150 200 250 300 350 400 450 500 550 Abundance #23027: Docosa-2,6,10,14,18-pentaen-22-al, 2,6,10,15,18-pe... 69 A)...... A)M A........ A I I I I I I r I I I I 11 fd ,I‘ I 1

33.60 33.80 34.00 34.20 34.40 5000 41 m/z 95.00 15.69%

111136 । - " 1,11' ,41,4,761192217.247273, 315341 ,384 3i ’1111’11 * ’ ’ I 1 ’’ I’ /z-> 0 50 100 150 200 250 300 350 400 450 500 550 Abundance #114263: Squalene ............... I.................. 69 33.60 33.80 34.00 34.20-34.40 m/z 136.00 14.42%

5000

41 95 137 ,। । j, i । T (Ad „ J ,163191 231 273299 341367 410 ................ T——r । । । i i । i i i i । । । r i j i i i i । i —i i f j i i i i । i i 1* । i i i । । i i । । । "r I 1 I I : I I I I I I > I I I I I I I I I I I

m/z--> 0 150 100 150 200 250 300 350 400 450 500 550 33.60 33.80 34.00 34.20 34.40

10610.D 050102.M Thu May 09 09:15:37 2002 Page 13

NYC-WTC_000045679

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