GCMS analysis results for sample AE10610, May 10 2002

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Laboratory report detailing GC/MS analysis of sample AE10610 including surrogate recovery data in May 2002.

NYC-WTC_000045662–000045681

Folder label: “GCMS X 5/3/02 A 5/7/02”

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NYC 9/11 Public Portal Document Library Search Compound Report Data File C:\MSDCHEM\l\DATA\050702\10610.D Vial: 13 Acq On 7 May 2002 10:55 pm Operator: Mclean Sample 5/3 kb Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title 508 Modified GC/MS scan Library C:\DATABASE\NIST98.L Peak Number 11 Cyclooct-4-en-l-ol, 8-iodo-.. Concentration Rank 11 R.T. EstConc Area Relative to ISTD R.T. 38.91 0.20 ug/L 174964 Perylene-dl2 34.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclooct-4-en-1-ol, 8-iodo-, ace... 294 C10H15IO2 1000197-11-8 9 2 (+)-2-Carene, 2-acetyl- 178 C12H180 1000151-09-7 3 Bicyclo[3.1.1]hept-3-ene-2-spiro... 194 C12H18O2 1000149-76-?/ 9 4 (4R,4Ar,5s)-5-isopropyl-4,4a-dim. . . 206 C15H26 055898-04-9 7 Abundance Scan 6098 (38.909 min): 10610.D (-6086) (-) m/z 43.10 100.00% 43

5000 81 107 $7 121 145 161 191 ....... . iM ill T I | > I I I | fFr I [‘T i l l 111 k,

—— 38.60 38.80 39.00 39.20 | 208 m/ Z 55.10 52.17% m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #7886: Cyclooct-4-en-1-ol, 8-iodo-, acetate 43 107 79 5000 'I ' ‘ F1 1 1 ' I 167 38.60 38.80 39.00 39.20 125 m/z 107.10 48.00% 27

m/z-> 57 _L । 11101Tl.li.. ii1"., II I1 1 1 'T 20 40 60 W 80 . ।

100 120 — 149 ‘T1 *1 1 ■ [ । 183196210 140 160 180 200 220 240 260 280 234 251 294 । 1 1 | 1 1 1 । | 1 1 । । | 1 ' r । |

Abundance #4522: (+)-2-Carene, 2-acetyl- 43 1 I ' 1 1 TTI 38.60 38.80 39.00 39.20 5000 m/ Z 41.20 46.96%

77 93 107 121 135 163 ,78 /z—> 20 44 63.11149 1 ............................ 40 I i 1 r । Tii । | i ill । II r r | I i i l । if rrB r i l | I i । i | > i i i [ i 11,TTV| ■ [ I l r | | IT’I 1T 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #371: Bicyclo[3.1.1]hept-3-ene-2-spiro-4'-(1 ',3'-dioxane),... * 1 i 1 ' 1 1 i ' 1 1 1 ' ' ' I ' 1 1 ' I 29 38.60 38.80 39.00 39.20 m/z 81.10 46.26% 91 5000 105 131 77

TT 44ARA44 (1,1186,111.761,179194 . ' i ■ ' ■ ■ । 11'' i ,,......... ,1,1, , . . ............ m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 38.60 38.80 39.00 39.20

10610.D 050102.M Thu May 09 09:15:40 2002 Page 14

NYC-WTC_000045680

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