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GCMS calibration data for volatile organic compounds, May 2002

Machine-extracted title · confidence 100%

Calibration run records for gas chromatography-mass spectrometry analysis of volatile organic compounds in water samples.

NYC-WTC_000044792–000044795

Folder label: “GCMS X 4/29/02 A 5/3/02

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NYC 9/11 Public Portal Document Lat.OIl KepOIC (QT Reviewed) Data File C:\HPCHEM\1\DATA\MAY0 6 02\CAL8 0A.D Vial: 2 Acq On 7 May 2002 6:45 pm Operator: Sample GC/MS SCAN 4/29 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 9 9:36 2002 Quant Results File: GCMS0507.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0507.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Tue May 07 08:24:38 2002 Response via : Initial Calibration DataAcq Meth : GCMS0507

Compound R.T. Qlon Response Cone Unit Qvalue

35) Anthracene 25.79 178 2639609 79.27 ug/1 100 36) Di-n-butylphthalate 27.56 14 9 3297974 79.85 ug/1 99 37) Fluoranthene 29.28 202 2514373 78.64 ug/1 97 3 9) Pyrene 29.95 202 2327075 85.35 ug/1 97 40) Butylbenzylphthalate 32.09 149 1166056 84.03 ug/1 93 41) Benzo(a)anthracene 33.59 228 1685901 80.18 ug/1 100 42) Bis(2-ethylhexyl)phthalate 33.87 149 1494433 81.20 ug/1 99 43) Chrysene 33.73 228 1663691 79.25 ug/1 100 45) Di-n-Octylphthalate 35.61 149 2152763 83.74 ug/1 # 95 46) Benzo(b)fluoranthene 36.70 252 1397546 79.24 ug/1 98 47) Benzo(k)fluoranthene 36.77 252 1526966 81.79 ug/1 98 48) Benzo(a)pyrene 37.69 252 1296429 81.34 ug/1 99 49) Indeno(1,2,3-cd)pyrene 41.98 276 1232151m 81.39 ug/1 50) Dibenz(a,h)anthracene 42.04 278 984079 81.58 ug/1 99 51) Benzo(g,h,i)perylene 43.21 276 967413 79.87 ug/1 99

(#) = qualifier out of range (m) = manual integration CAL80A.D GCMS0507.M Thu May 09 09:36:19 2002 Page 2

NYC-WTC_000044794

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NYC-WTC_000044794Source: NYC Law Department, mirrored locally

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