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GCMS reference results for VOCs, sample AE12535, June 2002

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Laboratory report showing GCMS reference analysis data for volatile organic compounds in sample AE12535 on June 3-4, 2002.

NYC-WTC_000014624–000014631

Folder label: “GCMS X 5/28/02 A 6/4/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) Data File C:\HPCHEM\1\DATA\JUN0302\REFA2.D Vial: 15 Acq On 3 Jun 2002 11:00 pm Operator: Sample gc/ms scan 5/28 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jun 4 11:37 2002 Quant Results File: GCMS0531.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0531.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri May 31 09:43:55 2002 Response via : Initial Calibration DataAcq Meth : GCMS0531

Compound R.T. Qlon Response Cone Unit Qvalue 35) Anthracene 25.62 178 601080 14.05 ug/1 100 36) Di-n-butylphthalate 27.41 149 870851 16.57 ug/1 99 37) Fluoranthene 29.11 202 677846 15.55 ug/1 100 39) Pyrene 29.78 202 702933 18.04 ug/1 100 40) Butylbenzylphthalate 31.93 149 303565 15.22 ug/1 100 41) Benzo(a)anthracene 33.42 228 432836 15.14 ug/1 99 42) Bis(2-ethylhexyl)phthalate 33.71 149 383283 14.63 ug/1 99 43) Chrysene 33.54 228 467041 16.47 ug/1 100 45) Di-n-Octylphthalate 35.45 149 473940 12.72 ug/1 # 98 46) Benzo(b)fluoranthene 36.51 252 329166 15.23 ug/1 99 47) Benzo(k)fluoranthene 36.57 252 353750 15.79 ug/1 99 4 8) Benzo(a)pyrene 37.46 252 223268 10.69 ug/1 98 49) Indeno(1,2,3-cd) pyrene 41.61 276 247377 12.64 ug/1 99 50) Dibenz (a,h)anthracene 41.69 278 213967 13.89 ug/1 97 51) Benzo(g,h,i)perylene 42.80 276 222836 13.96 ug/1 100

(#) = qualifier out of range (m) = manual integration REFA2.D GCMS0531.M Tue Jun 04 11:39:08 2002 Page 2

NYC-WTC_0000 14630

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NYC-WTC_000014630Source: NYC Law Department, mirrored locally

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