GCMS reference results for VOCs, sample AE12535, June 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\JUNO3O2\REFA2.D Vial: 15 Acq On 3 Jun 2002 11:00 pm Operator: Sample gc/ms scan 5/28 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jun 4 11:37 2002 Quant Results File: GCMS0531.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0531.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri May 31 09:43:55 2002 Response via : Initial Calibration DataAcq Meth : GCMS0531

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 12.07 152 485220 40.00 ug/1 0.00 10) Naphthalene-d8 15.70 136 1956954 40.00 ug/1 -0.02 17) Acenaphthene-diO 20.99 164 941684 40.00 ug/1 0.00 30) Phenanthrene-diO 25.43 188 1458766 40.00 ug/1 0.00 38) Chrysene-dl2 33.48 240 868326 40.00 ug/1 -0.03 44) Perylene-dl2 37.66 264 512230 40.00 ug/1 -0.03 System Monitoring Compounds 28) TCMX 23.13 209 183507 :28.17 ug/L -0.02 Spiked Amount 40.000 Recovery 70.43% Target Compounds Qvalue 2) N-nitrosodimethylamine 5.73 74 129668 8.73 ug/1 98 3) bis(2-Chloroethyl)ether 11.47 93 253867 13.08 ug/1 99 4) 1,3-Dichlorobenzene 11.97 146 220138 11.42 ug/1 100 5) 1,4-Dichlorobenzene 12.11 146 230715 11.05 ug/1 99 6) 1,2-Dichlorobenzene 12.63 146 229602 12.49 ug/1 99 7) 2,2’-oxybis(1-Chloropropan 12.95 45 414037 13.65 ug/1 98 8) N-Nitrosodi-n-propylamine 13.34 70 179447 13.38 ug/1 100 9) Hexachloroethane 13.48 117 73244 8.88 ug/1 96 11) Nitrobenzene 13.74 77 240059 13.29 ug/1 96 12) 1sophorone 14.39 82 514520 15.18 ug/1 99 13) bis(2-Chloroethoxy)methane 15.08 93 305815 13.73 ug/1 99 14) 1,2,4-Trichlorobenzene 15.59 180 191032 12.59 ug/1 98 15) Naphthalene 15.75 128 753074 14.62 ug/1 99 16) Hexachiorobutadiene 16.30 225 70078 10.49 ug/1 99 18) Hexachlorocyclopentadiene 18.50 237 11338 1.96 ug/1 96 19) 2-Chloronaphthalene 19.25 162 394087 15.71 ug/1 99 20) Dimethylphthalate 20.35 163 485591 15.23 ug/1 99 21) 2,6-Dinitrotoluene 20.56 165 98151 13.63 ug/1 97 2 2) Acenaphthylene 20.52 152 611007 13.58 ug/1 99 •23) Acenaphthene 21.09 153 420200 15.50 ug/1 100 24) 2,4-Dinitrotoluene 21.73 165 124209 14.74 ug/1 98 25) Diethylphthalate 22.48 149 496940 16.83 ug/1 99 26) 4-Chlorophenylphenylether 22.63 204 222343 15.83 ug/1 99 27) Fluorene 22.60 166 464027 16.85 ug/1 99 29) Azobenzene 23.10 77 510839 14.01 ug/L 97 31) N-Nitrosodiphenylamine 23.02 168 164792 15.47 ug/1 96 32) 4-Bromophenylphenylether 24.10 248 110738 15.13 ug/1 96 3 3) Hexachlorobenzene 24.52 284 132123 16.48 ug/1 96 34) Phenanthrene 25.49 178 664601 16.21 ug/1 100 (#) = qualifier out of range (m) = manual integration REFA2.D GCMS0531.M Tue Jun 04 11:39:07 2002 Page 1

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