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GCMS calibration results for sample AE10431, May 2002

Machine-extracted title · confidence 100%

Calibration data report for gas chromatography mass spectrometry analysis of sample AE10431 conducted in May 2002.

NYC-WTC_000045202–000045205

Folder label: “GCMS X 5/2/02 A 5/11/02

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NYC 9/11 Public Portal Document x uua CAt CL L L 011 Keport (QT Reviewed) Data File C:\HPCHEM\l\DATA\MAY1002\CAL80.D Vial: 24 Acq On 11 May 2002 12:31 pm Operator: Sample Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 15 14:59 2002 Quant Results File: GCMS0510.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0510.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed May 15 14:56:50 2002 Response via : Initial Calibration DataAcq Meth : GCMS0507

Compound R.T. Qlon Response Cone Unit Qvalue 35) Anthracene 25.76 178 2650964 78.66 ug/1 100 36) Di-n-butylphthalate 27.53 149 3305582 79.08 ug/1 100 37) Fluoranthene 29.26 202 2610351 80.68 ug/1 99 3 9) Pyrene 29.93 202 2465093 79.11 ug/1 94 40) Butylbenzylphthalate 32.07 149 1273061 80.27 ug/1 93 41) Benzo(a)anthracene 33.57 228 1943606 80.88 ug/1 99 42) Bis(2-ethylhexyl)phthalate 33.85 149 1625497 77.28 ug/1 99 43) Chrysene 33.71 228 1879682 78.34 ug/1 99 45) Di-n-Octylphthalate 35.59 149 2391958 81.65 ug/1 # 97 46) Benzo(b)fluoranthene 36.69 252 1601987 79.70 ug/1 97 47) Benzo(k)fluoranthene 36.76 252 1563798 73.50 ug/1 97 48) Benzo(a)pyrene 37.67 252 1471307 81.00 ug/1 99 49) Indeno(1,2,3-cd)pyrene 41.95 276 1411413 81.80 ug/1 99 50) Dibenz(a,h)anthracene 42.02 278 1109433 80.71 ug/1 99 51) Benzo(g,h,i)perylene 43.18 276 1106285m 80.15 ug/1

(#) = qualifier out of range (m) = manual integration CAL80.D GCMS0510.M Wed May 15 15:00:10 2002 Page 2

NYC-WTC_000045204

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NYC-WTC_000045204Source: NYC Law Department, mirrored locally

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