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GCMS calibration results for sample AE09447, May 2002

Machine-extracted title · confidence 100%

GCMS calibration report for sample AE09447 showing recovery percentages for various compounds from May 8, 2002.

NYC-WTC_000045411–000045414

Folder label: “GCMS X 5/3/02 A 5/8/02

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NYC 9/11 Public Portal Document

1 Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\l\DATA\MAY0802\CAL80.D Vial: 2 Acq On 8 May 2002 10:35 am Operator: Sample Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 9 14:28 2002 Quant Results File: GCMS0507.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0507.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Thu May 09 14:27:53 2002 Response via : Initial Calibration DataAcq Meth : GCMS0507

Compound R.T. Qlon Response Cone Unit Qvalue 35) Anthracene 25.79 178 2615089 79.71 ug/1 100 36) Di-n-butylphthalate 27.56 149 3244478 79.73 ug/1 99 37) Fluoranthene 29.28 202 2513497 79.80 ug/1 99 3 9) Pyrene 29.96 202 2351839 83.39 ug/1 95 40) Butylbenzylphthalate 32.08 149 1204234 83.89 ug/1 94 41) Benzo(a)anthracene 33.59 228 1756904 80.77 ug/1 100 42) Bis(2-ethylhexyl)phthalate 33.86 149 1542227 81.01 ug/1 100 43) Chrysene 33.72 228 1729776 79.65 ug/1 99 45) Di-n-Octylphthalate 35.61 149 2269995 82.12 ug/1 # 94 46) Benzo(b)fluoranthene 36.70 252 1438644 75.86 ug/1 98 47) Benzo(k)fluoranthene 36.77 252 1540187 76.73 ug/1 98 48) Benzo(a)pyrene 37.69 252 1387072 80.94 ug/1 98 49) Indeno(1,2,3-cd)pyrene 41.98 276 1361542 83.64 ug/1 98 50) Dibenz(a,h)anthracene 42.05 278 1088034 83.89 ug/1 99 51) Benzo(g,h,i)perylene 43.21 276 1068605 82.05 ug/1 98

(#) = qualifier out of range (m) = manual integration CAL80.D GCMS0507.M Thu May 09 14:28:31 2002 Page 2

NYC-WTC_000045413

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NYC-WTC_000045413Source: NYC Law Department, mirrored locally

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