Gas chromatography-mass spectrometry calibration run showing retention times and mass response for six deuterated reference standards and TCMX, completed May 4, 2002.
NYC-WTC_000023014–000023016Folder label: “GCMS X 5/8/02 A 5/9/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File C:\HPCHEM\l\DATA\MAY0302\CAL40 .D Vial: 100 Acq On 4 May 2002 4:33 pm Operator: Sample Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 7 14:21 2002 Quant Results File: GCMS0501.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed May 01 10:40:31 2002 Response via : Initial Calibration DataAcq Meth : GCMS0501
Compound R.T. Qlon Response Cone Unit Qvalue 35) Anthracene 25.78 178 1392726 40.79 ug/1 100 36) Di-n-butylphthalate 27.55 149 1807725 40.77 ug/1 100 37) Fluoranthene 29.28 202 1363932 42.10 ug/1 98 3 9) Pyrene 29.94 202 1267185 41.02 ug/1 99 40) Butylbenzylphthalate 32.08 149 675641 40.75 ug/1 98 41) Benzo(a)anthracene 33.59 228 982052 40.86 ug/1 99 42) Bis(2-ethylhexyl)phthalate 33.86 149 892019 41.81 ug/1 99 43) Chrysene 33.72 228 968584 41.44 ug/1 99 45) Di-n-Octylphthalate 35.61 149 1295588 39.49 ug/1 # 97 46) Benzo(b)fluoranthene 36.70 252 838452 41.41 ug/1 98 47) Benzo(k)fluoranthene 36.76 252 877371 41.87 ug/1 99 48) Benzo(a)pyrene 37.68 252 738736 39.63 ug/1 99 49) Indeno(1,2,3-cd)pyrene 41.97 276 693578 44.20 ug/1 97 50) Dibenz(a,h)anthracene 42.03 278 550789 44.38 ug/1 99 51) Benzo(g,h,i)perylene 43.19 276 551649 45.92 ug/1 99
(#) = qualifier out of range (m) = manual integration CAL40.D GCMS0501.M Tue May 07 14:24:56 2002 Page 2
NYC-WTC_000023015
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NYC-WTC_000023017
Laboratory report detailing gas chromatography mass spectrometry analysis of sample AE09570 conducted on May 14, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000022757
Reviewed data file listing retention times and response factors for deuterated internal standards.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000044257
Calibration record for GCMS analysis using standard compounds, generated on April 26, 2002, to ensure instrument accuracy.
1 shared topics · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043530
Calibration table excerpt from GCMS analysis of sample CAL20 showing surrogate recovery data from April 18, 2002.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000049405
Calibration report detailing response factors for multiple analytes used in the analysis of sample AE08971.
1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043536
Calibration table excerpt from GCMS analysis of sample REFA1 showing surrogate recovery data from April 19, 2002.
1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000011080
Calibration table listing retention times and concentrations for TCLP method analysis in March 2002.
1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000011121
Laboratory report showing GC/MS calibration data and surrogate recovery for sample AE03077 on March 22, 2002.
1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000011189
Laboratory report showing GC/MS calibration data and surrogate recovery for sample AE03182 on March 22, 2002.
1 shared topics · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000011132
Laboratory report showing GC/MS calibration data and surrogate recovery for sample AE03078 on March 22, 2002.
1 shared topics · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000059687
Gas chromatography-mass spectrometry analysis of sample AE01156 conducted March 29, 2002, showing surrogate standard 2,4-DDD recovery.
1 shared topics · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000011174
Laboratory report showing GC/MS calibration data and surrogate recovery for sample AE03181 on March 22, 2002.
1 shared topics · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000022961
Department of Environmental Protection administrative record sheet for World Trade Center site activities dated May 2002.
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NYC-WTC_000022962
Fragmentary record containing a document identifier and date from the DEP GCMS analysis series.
Filed in the same folder
NYC-WTC_000022965
Laboratory report of a GCMS blank run conducted on May 14, 2002, showing non-detect results for various compounds.
Filed in the same folder
NYC-WTC_000022990
Laboratory report documenting GCMS calibration verification analysis conducted on May 14, 2002.
Filed in the same folder
NYC-WTC_000022994
Laboratory report of GCMS reference standard analysis conducted on May 14, 2002, showing recovery percentages.
Filed in the same folder