Calibration record for GCMS analysis using standard compounds, generated on April 26, 2002, to ensure instrument accuracy.
NYC-WTC_000044257–000044259Folder label: “GCMS X 4/23/02 A 4/26/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File C:\HPCHEM\l\DATA\MAY0102\CAL40.D Vial: 2 Acq On 1 May 2002 8:59 am Operator: Sample Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 1 11:37 2002 Quant Results File: GCMS0501.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed May 01 10:40:31 2002 Response via : Initial Calibration DataAcq Meth : GCMS0501
Compound R.T. Qlon Response Cone Unit Qvalue
35) Anthracene 25.78 178 1170690 41.89 ug/1 99 36) Di-n-butylphthalate 27.55 149 1475858 40.67 ug/1 100 37) Fluoranthene 29.28 202 1113743 42.00 ug/1 98 39) Pyrene 29.95 202 1039971 38.87 ug/1 97 40) Butylbenzylphthalate 32.08 149 567825 39.54 ug/1 100 41) Benzo(a)anthracene 33.59 228 849777 40.82 ug/1 99 42) Bis(2-ethylhexyl )phthalate 33.86 149 736522 39.86 ug/1 100 43) Chrysene 33.72 228 832130 41.11 ug/1 99 45) Di-n-Octylphthalate 35.60 149 1128952 38.81 ug/1 99 46) Benzo(b)fluoranthene 36.70 252 753855 42.00 ug/1 98 47) Benzo(k)fluoranthene 36.76 252 778571 41.91 ug/1 100 48) Benzo(a)pyrene 37.68 252 671925 40.66 ug/1 99 49) Indeno(1,2,3-cd)pyrene 41.97 276 602193 43.28 ug/1 98 50) Dibenz(a,h)anthracene 42.04 278 478110 43.46 ug/1 100 51) Benzo(g,h,i)perylene 43.20 276 461406 43.32 ug/1 99
(#) = qualifier out of range (m) = manual integration CAL40.D GCMS0501.M Wed May 01 11:39:55 2002 Page 2
NYC-WTC_000044258
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NYC-WTC_000043530
Calibration table excerpt from GCMS analysis of sample CAL20 showing surrogate recovery data from April 18, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043536
Calibration table excerpt from GCMS analysis of sample REFA1 showing surrogate recovery data from April 19, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023014
Gas chromatography-mass spectrometry calibration run showing retention times and mass response for six deuterated reference standards and TCMX, completed May 4, 2002.
1 shared topics · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023017
Laboratory report detailing gas chromatography mass spectrometry analysis of sample AE09570 conducted on May 14, 2002.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000022757
Reviewed data file listing retention times and response factors for deuterated internal standards.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000049405
Calibration report detailing response factors for multiple analytes used in the analysis of sample AE08971.
1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000011080
Calibration table listing retention times and concentrations for TCLP method analysis in March 2002.
1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000011121
Laboratory report showing GC/MS calibration data and surrogate recovery for sample AE03077 on March 22, 2002.
1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000011189
Laboratory report showing GC/MS calibration data and surrogate recovery for sample AE03182 on March 22, 2002.
1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000059687
Gas chromatography-mass spectrometry analysis of sample AE01156 conducted March 29, 2002, showing surrogate standard 2,4-DDD recovery.
1 shared topics · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000011132
Laboratory report showing GC/MS calibration data and surrogate recovery for sample AE03078 on March 22, 2002.
1 shared topics · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000011200
Laboratory report showing GC/MS calibration data and surrogate recovery for sample AE03183 on March 22, 2002.
1 shared topics · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000044239
Single-page administrative log from DEP Box 25 covering GCMS X analyses dated between April 23 and April 26, 2002.
Filed in the same folder
NYC-WTC_000044240
Fragmented page from a GCMS record series dated between April 23 and April 26, 2002, likely containing analytical data.
Filed in the same folder
NYC-WTC_000044245
Laboratory report of a GCMS blank analysis (Sample AE07484) conducted on May 2, 2002, checking for background contamination.
Filed in the same folder
NYC-WTC_000044253
Calibration report listing quantified values for various organic compounds including nitrosamines and chlorobenzenes used for instrument verification.
Filed in the same folder
NYC-WTC_000044260
Reference report listing expected values for organic compounds including nitrosamines and chlorobenzenes used to validate analytical results.
Filed in the same folder