GCMS calibration results for sample AE09447, May 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\MAY0 8 02\CAL8 0.D Vial: 2 Acq On 8 May 2002 10:35 am Operator: Sample Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 9 14:28 2002 Quant Results File: GCMS0507.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0507.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Thu May 09 14:27:53 2002 Response via : Initial Calibration DataAcq Meth : GCMS0507

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.20 152 475841 40.00 ug/1 0.00 10) Naphthalene-d8 15.83 136 1717575 40.00 ug/1 0.00 17) Acenaphthene-dlO 21.14 164 926733 40.00 ug/1 0.00 30) Phenanthrene-diO 25.57 188 1314190 40.00 ug/1 0.00 38) Chrysene-dl2 33.65 240 836783 40.00 ug/1 0.01 44) Perylene-dl2 37.86 264 529012 40.00 ug/1 0.00

System Monitoring Compounds 2 8) TCMX 23.27 209 43728 9.49 ug/L 0.00 Spiked Amount 10.000 Recovery = 94.90%

Target Compounds S//07 Qvalue 2) N-nitroso-dimethyl amine 5.84 74 923038 77.01 ug/1 97 3) bis(2-Chloroethyl)ether 11.59 93 1198622 77.11 ug/1 95 4) 1,3-Dichlorobenzene 12.10 146 1164615 78.98 ug/1 97 5) 1,4-Dichlorobenzene 12.24 146 1273389 78.93 ug/1 99 6) 1,2-Dichlorobenzene 12.76 146 1099713 78.32 ug/1 99 7) 2,21-oxybis(1-Chloropropan 13.08 45 2269143 75.29 ug/1 98 8) N-Nitroso-di-n-propylamine 13.47 70 855965 77.08 ug/1 96 9) Hexachloroethane 13.60 117 447242 77.92 ug/1 95 11) Nitrobenzene 13.88 77 1106235 79.33 ug/1 95 12) Isophorone 14.52 82 2134474 78.09 ug/1 96 13) bis(2-Chloroethoxy)methane 15.21 93 1386006 78.27 ug/1 100 14) 1,2,4-Trichlorobenzene 15.71 180 957108 80.26 ug/1 98 15) Naphthalene 15.89 128 2803834 79.34 ug/1 99 16) Hexachlorobutadiene 16.43 225 450017 81.52 ug/1 100 18) Hexachlorocyclopentadiene 18.63 237 384128 81.79 ug/1 100 19) 2-Chloronaphthalene 19.40 162 1607382 79.39 ug/1 97 20) Dimethylphthalate 20.50 163 2033455 79.76 ug/1 100 21) 2,6-Dinitrotoluene 20.72 165 466125 85.49 ug/1 89 22) Acenaphthylene 20.67 152 2850548 79.01 ug/1 99 23) Acenaphthene 21.24 153 1709291 79.48 ug/1 99 24) 2,4-Dinitrotoluene 21.88 165 516476 87.88 ug/1 # 88 25) Diethylphthalate 22.63 149 1810841 79.31 ug/1 99 26) 4-Chlorophenyl-phenylether 22.78 204 906384 80.31 ug/1 96 27) Fluorene 22.75 166 1802969 79.51 ug/1 100 29) Azobenzen/ 1,2-Diphenylhyd 23.25 77 2142343 75.79 ug/L # 94 31) N-Nitrosodiphenylamine 23.17 168 670834 81.72 ug/1 # 90 32) 4-Bromophenyl-phenylether 24.25 248 525206 80.82 ug/1 95 33) Hexachlorobenzene 24.68 284 595013 80.14 ug/1 100 34) Phenanthrene 25.66 178 2507542 79.52 ug/1 100

(#) = qualifier out of range (m) = manual integration CAL80.D GCMS0507.M Thu May 09 14:28:30 2002 Page 1

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