GCMS reference analysis results for sample AE09447, May 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\l\DATA\MAY0802\REFl.D Vial: 4 Acq On 8 May 2002 1:30 pm Operator : Sample GC/MS SCAN 5/3 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 9 14:30 2002 Quant Results File: GCMS0507.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0507.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Thu May 09 14:27:53 2002 Response via : Initial Calibration DataAcq Meth : GCMS0507

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.19 152 456825 40.00 ug/1 0.00 10) Naphthalene-d8 15.83 136 1669159 40.00 ug/1 0.00 17) Acenaphthene-diO 21.13 164 915182 40.00 ug/1 0.00 30) Phenanthrene-diO 25.58 188 1264751 40.00 ug/1 0.00 38) Chrysene-dl2 33.63 240 708599 40.00 ug/1 0.00 44) Perylene-dl2 37.86 264 409153 40.00 ug/1 0.00

System Monitoring Compounds 2 8) TCMX 23.27 209 40671 8.93 ug/L 0.00 Spiked Amount 10.000 Recovery 89.30%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.83 74 134661 11.70 ug/1 97 3) bis(2-Chloroethyl)ether 11.59 93 255378 17.11 ug/1 97 4) 1,3-Dichlorobenzene 12.09 146 175494 12.40 ug/1 96 5) 1,4-Dichlorobenzene 12.24 146 190190 12.28 ug/1 98 6) 1,2-Dichlorobenzene 12.75 146 192207 14.26 ug/1 98 7) 2,21 -oxybis(1-Chloropropan 13.07 45 526496 18.20 ug/1 98 8) N-Nitroso-di-n-propylamine 13.46 70 193521 18.15 ug/1 99 9) Hexachloroethane 13.60 117 41877 7.60 ug/1 95 11) Nitrobenzene 13.87 77 230705 17.02 ug/1 98 12) Isophorone 14.52 82 544081 20.48 ug/1 97 13) bis(2-Chloroethoxy)methane 15.21 93 308471 17.92 ug/1 99 14) 1,2,4-Trichlorobenzene 15.71 180 162570 14.03 ug/1 99 15) Naphthalene 15.88 128 615082 17.91 ug/1 100 16) Hexachlorobutadiene 16.42 225 36102 6.73 ug/1 99 18) Hexachlorocyclopentadiene 18.62 237 13580 2.93 ug/1 97 19) 2-Chloronaphthalene 19.38 162 372721 18.64 ug/1 98 20) Dimethylphthalate 20.47 163 485759 19.29 ug/1 99 21) 2,6-Dinitrotoluene 20.69 165 90422 16.79 ug/1 96 22) Acenaphthylene 20.66 152 594400 16.68 ug/1 100 23) Acenaphthene 21.23 153 392528 18.48 ug/1 99 24) 2,4-Dinitrotoluene 21.87 165 105201 18.13 ug/1 88 25) Diethylphthalate 22.61 149 474592 21.05 ug/1 99 26) 4-Chlorophenyl-phenylether 22.77 204 196220 17.61 ug/1 99 27) Fluorene 22.75 166 429656 19.19 ug/1 100 29) Azobenzen/ 1,2-Diphenylhyd 23.23 77 479114 17.16 ug/L 96 31) N-Nitrosodiphenylamine 23.16 168 162664 20.59 ug/1 93 32) 4-Bromophenyl-phenylether 24.23 248 110270 17.63 ug/1 98 33) Hexachlorobenzene 24.67 284 130375 18.25 ug/1 99 34) Phenanthrene 25.64 178 579358 19.09 ug/1 100

(#) = qualifier out of range (m) = manual integration REFl.D GCMS0507.M Thu May 09 14:31:37 2002 Page 1

NYC-WTC_000045417