GCMS reference standard report, May 6, 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\l\DATA\MAY0302\REFl.D Vial: 4 Acq On 3 May 2002 4:57 pm Operator: Sample GC/MS SCAN 4/24 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 6 9:37 2002 Quant Results File: GCMS0501.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed May 01 10:40:31 2002 Response via : Initial Calibration DataAcq Meth : GCMS0501

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.19 152 492180 40.00 ug/1 -0.02 10) Naphthalene-d8 15.83 136 1800091 40.00 ug/1 -0.02 17) Acenaphthene-diO 21.14 164 956077 40.00 ug/1 -0.01 30) Phenanthrene-diO 25.58 188 1336696 40.00 ug/1 -0.01 38) Chrysene-dl2 33.65 240 775834 40.00 ug/1 -0.02 44) Perylene-dl2 37.87 264 455026 40.00 ug/1 -0.01

System Monitoring Compounds 28) TCMX 23.28 209 38410 8.25 ug/L -0.01 Spiked Amount 10.000 Recovery = 82.50%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.84 74 157797 11.73 ug/1 100 3) bis(2-Chloroethyl)ether 11.59 93 287171 16.45 ug/1 98 4) 1,3-Dichlorobenzene 12.09 146 164128 10.70 ug/1 99 5) 1,4-Dichlorobenzene 12.24 146 179488 10.71 ug/1 98 6) 1,2-Dichlorobenzene 12.75 146 188493 12.97 ug/1 99 7) 2,21 -oxybis(1-Chloropropan 13.07 45 594283 16.47 ug/1 98 8) N-Nitroso-di-n-propylamine 13.46 . 70 221998 16.97 ug/1 100 9) Hexachloroethane 13.61 117 33259 5.28 ug/1 92 11) Nitrobenzene 13.87 77 236122 14.40 ug/1 99 12) Isophorone 14.52 82 616146 19.39 ug/1 99 13) bis(2-Chloroethoxy)methane 15.21 93 342059 16.96 ug/1 100 14) 1,2,4-Trichlorobenzene 15.71 180 154156 12.64 ug/1 98 15) Naphthalene 15.89 128 645468 17.13 ug/1 100 16) Hexachlorobutadiene 16.43 225 25651 4.58 ug/1 98 18) Hexachlorocyclopentadiene 18.63 237 14760 3.05 ug/1 99 19) 2-Chloronaphthalene 19.39 162 382368 18.11 ug/1 99 20) Dimethylphthalate 20.49 163 502615 18.70 ug/1 100 21) 2,6-Dinitrotoluene 20.70 165 75719 12.97 ug/1 99 22) Acenaphthylene 20.66 152 636662 16.76 ug/1 100 23) Acenaphthene 21.23 153 409571 18.38 ug/1 100 24) 2,4-Dinitrotoluene 21.87 165 80079 12.79 ug/1 94 25) Diethylphthalate 22.62 149 491815 20.17 ug/1 99 26) 4-Chlorophenyl-phenylether 22.77 204 197139 17.09 ug/1 98 27) Fluorene 22.75 166 450892 18.98 ug/1 99 29) Azobenzen/ 1,2-Diphenylhyd 23.24 77 527334 16.10 ug/L 98 31) N-Nitrosodiphenylamine 23.16 168 171097 19.31 ug/1 96 32) 4-Bromophenyl-phenylether 24.24 248 111125 17.11 ug/1 97 33) Hexachlorobenzene 24.68 284 134808 18.59 ug/1 100 34) Phenanthrene 25.65 178 601613 18.57 ug/1 100

(#) = qualifier out of range (m) = manual integration REFl.D GCMS0501.M Mon May 06 09:39:07 2002 Page 1

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