GCMS reference standard results, sample AE06048, May 3, 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\l\DATA\MAY0202\REFA2.D Vial: 13 Acq On 3 May 2002 2:38 am Operator: Sample GC/MS SCAN 4/22 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 3 9:48 2002 Quant Results File: GCMS0501.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed May 01 10:40:31 2002 Response via : Initial Calibration DataAcq Meth : GCMS0501

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.19 152 393964 40.00 ug/1 -0.02 10) Naphthalene-d8 15.83 136 1445556 40.00 ug/1 -0.02 17) Acenaphthene-diO 21.14 164 780573 40.00 ug/1 -0.01 30) Phenanthrene-diO 25.58 188 1039953 40.00 ug/1 -0.01 38) Chrysene-dl2 33.65 240 652878 40.00 ug/1 -0.02 44) Perylene-dl2 37.87 264 421246 40.00 ug/1 -0.01

System Monitoring Compounds 28) TCMX 23.27 209 38206 10.05 ug/L -0.02 Spiked Amount 10,000 Recovery = 100.50%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.84 74 118875 11.04 ug/1 98 3) bis(2-Chloroethyl)ether 11.59 93 226799 16.23 ug/1 98 4) 1,3-Dichlorobenzene 12.09 146 189084 15.40 ug/1 99 5) 1,4-Dichlorobenzene 12.24 146 198452 14.79 ug/1 99 6) 1,2-Dichlorobenzene 12.75 146 191692 16.48 ug/1 99 7) 2,21 -oxybis(1-Chloropropan 13.07 45 483273 16.73 ug/1 99 8) N-Nitroso-di-n-propylamine 13.46 70 176562 16.86 ug/1 100 9) Hexachloroethane 13.61 117 55821 11.08 ug/1 95 11) Nitrobenzene 13.87 77 183095 13.91 ug/1 97 12) Isophorone 14.52 82 504504 19.77 ug/1 99 13) bis(2-Chloroethoxy)methane 15.21 93 273541 16.89 ug/1 100 14) 1,2,4-Trichlorobenzene 15.71 180 161359 16.48 ug/1 98 15) Naphthalene 15.89 128 558496 18.45 ug/1 99 16) Hexachlorobutadiene 16.44 225 58451 12.99 ug/1 99 18) Hexachlorocyclopentadiene 18.63 237 19560 4.94 ug/1 96 19) 2-Chloronaphthalene 19.39 162 334042 19.38 ug/1 99 20) Dimethylphthalate 20.49 163 418598 19.08 ug/1 99 21) 2,6-Dinitrotoluene 20.70 165 53234 11.17 ug/1 95 22) Acenaphthylene 20.66 152 513676 16.56 ug/1 99 23) Acenaphthene 21.23 153 343798 18.89 ug/1 98 24) 2,4-Dinitrotoluene 21.87 165 54752 10.71 ug/1 96 25) Diethylphthalate 22.62 149 409290 20.56 ug/1 100 26) 4-Chlorophenyl-phenylether 22.77 204 176941 18.79 ug/1 99 27) Fluorene 22.75 166 377847 19.48 ug/1 100 29) Azobenzen/ 1,2-Diphenylhyd 23.24 77 432511 16.18 ug/L 98 31) N-Nitrosodiphenylamine 23.16 168 113846 16.51 ug/1 96 32) 4-Bromophenyl-phenylether 24.24 248 99202 19.64 ug/1 97 33) Hexachlorobenzene 24.67 284 118775 21.05 ug/1 99 34) Phenanthrene 25.65 178 495791 19.67 ug/1 99

(#) = qualifier out of range (m) = manual integration REFA2.D GCMS0501.M Fri May 03 09:53:39 2002 Page 1

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