GCMS reference standard results, sample AE06048, May 3, 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\l\DATA\MAY0202\REFAl.D Vial: 12 Acq On 3 May 2002 1:38 am Operator : Sample GC/MS SCAN 4/22 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 3 9:45 2002 Quant Results File: GCMS0501.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed May 01 10:40:31 2002 Response via : Initial Calibration DataAcq Meth : GCMS0501

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.19 152 424488 40.00 ug/1 -0.02 10) Naphthalene-d8 15.83 136 1554682 40.00 ug/1 -0.02 17) Acenaphthene-diO 21.14 164 844477 40.00 ug/1 -0.01 30) Phenanthrene-diO 25.58 188 1181564 40.00 ug/1 -0.01 38) Chrysene-dl2 33.65 240 767587 40.00 ug/1 -0.02 44) Perylene-dl2 37.87 264 499211 40.00 ug/1 -0.01

System Monitoring Compounds 2 8) TCMX 23.28 209 40269 9.80 ug/L -0.01 Spiked Amount 10.000 Recovery = 98.00%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.84 74 130735 11.26 ug/1 98 3) bis(2-Chloroethyl)ether 11.59 93 248135 16.48 ug/1 98 4) 1,3-Dichlorobenzene 12.09 146 198497 15.00 ug/1 97 5) 1,4-Dichlorobenzene 12.24 146 210564 14.56 ug/1 100 6) 1,2-Dichlorobenzene 12.75 146 207332 16.54 ug/1 100 7) 2,2'-oxybis(1-Chloropropan 13.07 45 529704 17.02 ug/1 99 8) N-Nitroso-di-n-propylamine 13.46 70 195235 17.30 ug/1 99 9) Hexachloroethane 13.61 117 57397 10.57 ug/1 97 11) Nitrobenzene 13.88 77 197961 13.98 ug/1 98 12) Isophorone 14.52 82 539604 19.66 ug/1 99 13) bis(2-Chloroethoxy)methane 15.21 93 299266 17.18 ug/1 99 14) 1,2,4-Trichlorobenzene 15.71 180 172917 16.42 ug/1 99 15) Naphthalene 15.89 128 611203 18.78 ug/1 99 16) Hexachlorobutadiene 16.44 225 59715 12.34 ug/1 99 18) Hexachlorocyclopentadiene 18.63 237 18990 4.44 ug/1 96 19) 2-Chloronaphthalene 19.40 162 368623 19.77 ug/1 98 20) Dimethylphthalate 20.49 163 453614 19.11 ug/1 100 21) 2,6-Dinitrotoluene 20.70 165 56177 10.89 ug/1 96 22) Acenaphthylene 20.66 152 577356 17.20 ug/1 99 23) Acenaphthene 21.23 153 380340 19.32 ug/1 100 24) 2,4-Dinitrotoluene 21.87 165 58863 10.64 ug/1 96 25) Diethylphthalate 22.62 149 445314 20.68 ug/1 99 26) 4-Chlorophenyl-phenylether 22.77 204 193232 18.97 ug/1 98 27) Fluorene 22.75 166 417837 19.91 ug/1 99 29) Azobenzen/ 1,2-Diphenylhyd 23.24 77 473968 16.38 ug/L 98 31) N-Nitrosodiphenylamine 23.16 168 130032 16.60 ug/1 96 32) 4-Bromophenyl-phenylether 24.24 248 107771 18.78 ug/1 98 33) Hexachlorobenzene 24.68 284 129529 20.21 ug/1 100 34) Phenanthrene 25.65 178 552253 19.29 ug/1 99

(#) = qualifier out of range (m) = manual integration REFA1.D GCMS0501.M Fri May 03 09:46:35 2002 Page 1

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