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← Document results/DEP Box 25/GCMS X 4/29/02 A 5/3/02
Document / 8 pages

GCMS calibration table for TCLP analysis, April 2002

Machine-extracted title · confidence 100%

Calibration data file listing standard compounds and response factors for TCLP testing from late April 2002.

NYC-WTC_000044723–000044730

Folder label: “GCMS X 4/29/02 A 5/3/02

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Scanned page image, NYC-WTC_000044726
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Data File : C:\HPCHEM\1\DATA\APR2502\9336.D Vial: 13 Acq On : 26 Apr 2002 12:21 am Operator: Sample : gc/ms scan 4/18 fb Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.187 338 342 369 rVB 221665 523311 11.56% 2.280% 2 12.208 775 780 795 rBV 1328363 3141809 69.39% 13.691% 3 15.844 1170 1176 1193 rBV 2017681 4035492 89.13% 17.585% 4 21.150 1747 1754 1773 rBV 2207890 4527699 100.00% 19.730% 5 23.280 1977 1986 1992 rBV 187465 377580 8.34% 1.645%

6 25.584 2231 2237 2249 rBV2 1992265 4416420 97.54% 19.245% 7 25.722 2249 2252 2264 rVB 15983 45873 1.01% 0.200% 8 33.644 3108 3115 3135 rBV2 1497081 3386815 74.80% 14.758% 9 37.876 3567 3576 3595 rBV2 840627 2493773 55.08% 10.867%

Sum of corrected areas: 22948772

9336.D GCMS0412.M Fri Apr 26 07:55:21 2002

NYC-WTC_000044726

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NYC-WTC_000044726Source: NYC Law Department, mirrored locally

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