GCMS analysis results for sample AE09335, May 2002

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Laboratory report documenting GCMS analysis of sample AE09335 conducted on May 8, 2002.

NYC-WTC_000044672–000044699

Folder label: “GCMS X 4/29/02 A 5/3/02”

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NYC 9/11 Public Portal Document

Data File C:\MSDCHEM\1\DATA\050202\9335.D Vial: 13 Acq On 2 May 2002 9:27 pm Operator: Mclean Sample 4/29 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 13 Cyclopent[e]-1,3-oxazine, o.. Concentration Rank' 3

R.T. EstConc Area Relative to ISTD R.T.

36.39 3.19 ug/L 3754750 Perylene-dl2 34.73

Hit# of 5 Tentative ID MW MolForm CAS# Qual ,

1 Cyclopent[e]-1,3-oxazine, octahy... 216 C13H16N20 1000138-92-2 41 2 2-Hydroxy-6-heptadec-8Z,11Z,14Z-... 370 C24H3403 1000144-50-2/38 3 1-Cycloheptene-3-carboxamide, N-... 215 C14H17NO 1000159-24/4 20 4 Acetic acid, 2-acetoxymethyl-6-(... 326 C14H18N2O7 1000193-14-0 16 Abundance Scan 5670 (36.394 min): 9335.D (-5659) (-) m/z 215.20 100.00% 43 21 5 95 233 149 69 5000 121

355373 Kr Ti ■ "I ' [ ‘*

....... I AM 1 73191 A., 14, —ll 1 22 288 331 111 1′0011′101111110111111111011101111117117 36.00 36.20 36.40 36.60 36.80 m/ z 43.20 91.01% 11" " I

N m/z-> :20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance> #86591: Cyclopent[e]-1,3-oxazine, octahydro-2-(phenylimino... 2 5

-PWWA—y 01

5000 135 36.00 36.20 36.40 36.60 36.80 41 93 m/ z 95.10 73.58% 65 118 11," 11 ’ ’1 (‘ ‘11’1 r 1" i " " r " ■ i V1 " I11 1 ' I " 1 1 I 1 " ' I1 FI7 I U I | I I I I | ! I I I I r, IT] m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #30975: 2-Hydroxy-6-heptadec-8Z,11 Z,14Z-trienylbenzoic acid 79 108 I 1 ' ’ 1 I ‘ ’ 1 1 1 1 ’ ’ 1 I ■ 1 ■ ' I ' ' 36.00 36.20 36.40 36.60 36.80

A 5000 m/ Z 81.10 70.27% 370 147

n/z-> LW— 173 T‘m—I"u—D011111110101111012011 —10—301001110m7 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance। #40480: 1-Cycloheptene-3-carboxamide, N-phenyl- MMAMAP III I II I I* * 93 36.00 36.20 36.40 36.60 36.80 215 m/z 233.20 69.86%

5000 67 41 172

/z-> 4 i11111111'i " '' i111 ■ i " ''i11 ■ • r 111111111r 1111 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 ................. A 36.00 36.20 36.40 36.60 36.80

9335.D 050102.M Mon May 06 13:59:57 2002 Page 18

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