GCMS sample analysis summary, May 7, 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\HPCHEM\1\DATA\MAY0302\8837.D Vial: 6 Acq On 3 May 2002 6:56 pm Operator: Sample RE-EXT. Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Butanamide Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T. 9.14 1.42 ug/1 99268 1,4-Dichlorobenzene-d4 12.19 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Butanamide 87 C4H9NO 000541-35-5 72 2 Amylene Hydrate 88 C5H120 000075-85-4 39 3 2-Hexanone, 3-hydroxy-3,5-dimethyl- 144 C8H1602 006321-14-8 39 4 2-Ogtanol, 2-methyl-_________________ 144 C9H20O 000628-44-4 38 Abundance/ Scan 447 (9.139 min): 8837.D (-) m/z 59.10 100.00% 59

5000 43 ■ ■ i r 1 ■ ' i r 1 1 1 1 1 1 1 1 i 1 r 1 ' i 1

............... . i । I I n । i i i r | I ! I I j t r i ..69.... 87...................... 153 m/z8.80 43.05 1 | ' । । । | | | 9.00 9.20 9.40 | I 38.21% | | | |I | । i I I | i i TT | i I I i | r I I I [ I I r i | i i i i I'll I I | I

m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #62880: Butanamide 44 59

J 5000 8.80 9.00 9.20 9.40 27 72 m/z 41.05 17.80% ■ i ■ ■ ■ ■ । ■ 11 1 11 1 1 1 | ' 1 । । 1 । 87 । । ■ ■ < ■ । । r ■ ■ i ■ ■ > ■ । । TT । । > । । । । । । । । । 1 i ■ ■ 1'■ । mlz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #62938: Amylene Hydrate 59 l l I I II I I I 1 '1-1 I 1 1 1 1 I 77 8.80 9 00 9.20 9.40 73 m/z 153.00 6.17% 5000 31 43

l-i-j-r Hh i11111 +L i । । iii IT । ' । ।11 I । । । । । । i । । । । । । । । n । i i । । । । i । i । । । i । । ri i r [ i'm- । i m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #8436: 2-Hexanone, 3-hydroxy-3,5-dimethyl- I I I [ III! | I I I I | I ■ ■ । ■ ■ ■ • । ■ 59 8.80 9.00 9.20 9.40 m/z 151.05 6.10% 5000 43 101 1111' ■ i11111, 1111 I | 1 ’ 69| । I I | 83 । [ i r [ | f | | 111 | I I "J '! | I I I | I | | | I | । । । । | i i i I I T I I I - “ I I f 1T T । i—| iiii ] I ‘ । i | i । r r—| I I I I 1 m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 8.80 9.00 9.20 9.40

8837.D GCMS0501.M Mon May 06 10:48:16 2002 Page 3

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