GCMS blank analysis report, May 6, 2002

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Library Search Compound Report

Data File C:\HPCHEM\l\DATA\MAY0602\LB.D Vial: 3 Acq On 6 May 2002 11:27 am Operator:’ Sample GC/MS SCAN 4/24 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 5 Isoetharine Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

29.01 0.60 ug/1 54596 Phenanthrene-dl0 25.58 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Isoetharine 239 C13H21NO3 000530-08-5 40 2 Furaltadone 324 C13H16N4O6 000139-91-3 39 3 Imidazole, 5-fluoro-4-methyl- 100 C4H5FN2 000000-00-0 38 4 Nimorazole 226 C9H14N4O3 006506-37-2 9 Abundance ? Scan 2616 (29.015 min): LB.D (-) m/z 100.05 100.00% 100

5000

| 1 I I-1 | । T i k V ) I I I I | I I i1 I T 43 55 70 28.60 28.80 29.00 29.20 29.40 87 m/ z m . . "+ii | I ‘ | l I l !'| I TT i 43.10 6.88%

1 m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #31749: Isoetharine 100 58 5000 ft A M WWN WA /WY | I iF i I । 1 i i । < Fi i । । i i f I I

28.60 28.80 29.00 29.20 29.40 m/z 101.15 6.58% 41 , 70 84 123 192 i1 ■ " r 1'11111 TTT-I-TTTTuuT ‘ । | ITT Fi | i i i r [ I i > i | i i i I | i i i i । i i i i | i i i । । I i i i | | | | | j

mlz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #46033: Furaltadone 100 28.60 28.80 29.00 29.20 29.40 5000 m/ z 41.05 4.79%

42 56 70 79 128 185 । । । । । ।1II i I । । ।' r । । i i 11111 r' i' " ' r 111111111111111111111*111111111111111111'11 [ I I I J m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #1440: Imidazole, 5-fluoro-4-methyl- 100 AMWAAMMARAMAN | I I I i | r I I I | I I | I j |' I | r | r r 28.60 28.80 29.00 29.20 29.40 m/z 42.15 4.22% 5000 42 72 52 — ! | ! ! ! 1______________________________________ m lihis i-p-r ' । । । [ । * i । । । । ( । [ i । । i । । i i i । i i i i । r i I i | I i i i । i ri i । i r FI mfe-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 28.60 28.80 29.00 29.20 29.40

LB.D GCMS0501.M Wed May 08 11:53:47 2002 Page 5

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