GCMS analysis results for sample AD30015, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

' 'Data File : C:\HPCHEM\l\DATA\DEC1801\30015.D Vial: 12 Acq On : 19 Dec 2001 2:50 am Operator: 209 GALOS Sample : gc/ms scan 12/11 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 4 Cyclohexanone, phenylhydrazone Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

25.12 0.26 ug/1 90866 Phenanthrene-dl0 24.97

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclohexanone, phenylhydrazone 188 C12H16N2 000946-82-7 50 2 1,4 -Naphthalenedione. 2-hydroxy-3-m 188 CHH803 000483-55-6 43 3 Phenanthre -diO 188 C14D10 001517-22-2 40 4 Pentacyclo [8.4.0.0(3,7) .0(4,14) .0(6 188 C14H20 000000-00-0 40 Abundance v Scan 2187 (25.119 min): 30015.D(-) m/z 18 710 100.00%| 1(18

5000- 94 64 80 146 160

m/z-> _____ 30 40 mPT -.. 444 40 52 50 60 —— — ITT 70 80 90 100 110 120 130 140 150 160 170 180 190 1170.1401 24.80 25.00 25.20 25.40 m/z 94.00 27.39% Abundance #19927: Cyclohexanone, phenylhydrazone 188 93

5000 24.80 25.00 25.20 25.40 65 77 106 m/z 9 .00 23.38% L 120 132 1451159 170 i • ■ ■ ■ i ■ 111" ’ i ■ ■ ■ ■ i ■ ■ ■ • । ■ TIT ri 11111 11 । «»>»11« TT m/z--> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #69174: 1.4-Naphthalenedione, 2-hydroxy-3-methyl- 188

24.80 25.00 25.20 25.40 5000- m/z 189.10 22.32%

77 105 131 160 50 115 ||. H I m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19958: Phenanthrene-d10 .... /........ 188 24.80 25.00 25.20 25.40 m/z 160.05 17.29% 5000-

80 94 160 “TTguP 66 - ------- 4 H m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 24.80 25.00 25.20 25.40

30015.D GCMS1126.M Tue Jan 15 15:38:00 2002 Page 4

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