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GCMS analysis results for sample AD24216, Nov 6 2001

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Laboratory report documenting GCMS analysis of sample AD24216 conducted on November 6, 2001, noting unknown compounds.

NYC-WTC_000067990–000068002

Folder label: “GCMS Scan X 10/10/01 An 11/1/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV0101\24215.D Vial: 2 Acq On : 1 Nov 2001 4:00 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr; 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Librai^f : C:\DATABASE\NBS75K.L Peak Number 4 Phenanthrene-dlO Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 25.03 20.00 ug/1 5517940 Phenanthrene-dl0 25.16 Hit# of/ 5 Tentative ID MW MolForm CAS# Qual 1 Phmanthrene-dlO 188 C14D10 001517-22-2 98 2 Airchracene-dlO- 188 C14D10 001719-06-8 83 3 Cyclohexanone, phenylhydrazone 188 C12H16N2i 000946-82-7 53 4/4-Fluoro-6-methyl-2-phenylpyrimidin 188 ClIH9FN2I ______ 000000-00-0 45 Scan 2177 (25.027 min): 24215.D (-) m/z 188.10 100.00%

5000 Hf”' T 80 94 160 24.60 24.80 25,00 25.20 25,40 11..,. 1,,, I,. 1111., 1111. , I .If?,, I ;-i|., .IJP, m/z 187.20 20.72% TTfe-> "to "ct'to "ro "m'iOo'i 10 W 'l^ 'l4o' 'i'ot ITO 17O w ' Wwjndance #19958: Phenanthrene-d10 US

5000 24.60 24.80 25.00 25.20 25.40 m/z 189.10 14.42% 80 94 160 66 4... ill-i.... . ........ nfe-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19957: Anthracene-dl 0- 118 T T T T 24.60 24.80 25.00 25.20 25.40 5000 m/z 184.10 13.41% fl 80 94 160

Ti/z-> .......... ..... I... ■!.„.......... 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 .. . Abundance #19927: Cyclohexanone, phenyihydrazone ................ \ .................. II8 24.60 24.80 25.00 25.20 25.40 93 “mTz 80.05 13.35% 5000- 65 77 106 145 I 159 170 . I'., I. T T ■nfe-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 24.60 24.80 25.00 25.20 25.40

24215.D NP103001.M Tue Nov 06 11:44:45 2001 Page 4

NYC-WTC_000068001

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NYC-WTC_000068001Source: NYC Law Department, mirrored locally

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