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GC/MS analysis results for sample AD23838, Nov 2 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23838 conducted on November 2, 2001, identifying unknown compounds.

NYC-WTC_000089346–000089365

Folder label: “GC/MS Scan 10/1/01

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Scanned page image, NYC-WTC_000089356
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT3001\23838.D Vial; 12 Acq On ; 31 Oct 2001 1;15 am Operator; 2 09 GT^LOS Sample ; gc/ms unknown Inst : GC/MS 209 Mise Multiplr; 1,00 MS Integration Params; LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title ; 209 625/TCLP calibration table Library ; C:\DATABASE\NBS75K.L ********************************************************* *i********** Peak Number 4 Phenanthrene-dlO Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T.

25.03 20.00 ug/1 6672640 Phenanthrene-dl0 25.17 Hit# of/ 5 Tentative ID MW MolForm CAS# Qual , 1 Phenanthrene-dlO 188 C14D10 001517-22-2 96 2 An^racene-dlO- 188 C14D10 001719-06-8 95 3 'clohexanone, phenylhydrazone 188 C12H16N2 000946-82-7 59 4 -Fluoro-6-methyl-2-phenyIpyrimidin 188 C11H9FN2 000000-00-0 45 ^buni ince Scan 2177 (25.027 min): 23838.D (-) m/z 188.10 100.00% 1I!8

5000

160 I 24,60 24.80 25,00 25,20 25.40 30 40 50 ' 60 70 ' 80 ' 90' 'l'oo' 11W 120 'iSO 140 'l50 leO 'iTO 'l80 1^ m/z 187.20 19.21% Abundance #19958: Phenanthrene-dlO 1$8

5000 i 24.60 24.80 25.00 25.20 25.40 m/z 189.10 15700% 80 94 160 66 Ti/z-> I " I' I 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 .. I....... K... Abundance #19957: Anthracene-d10- 1$8 ,2" , ■, 24.60 24.80 25.00 25.20 25.40 5000 m/z 184.10 13.44%

66 ’I’ 1® ,|| T Tife-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19927; Cyclohexanone, phenylhydrazone T T T —1B8- 24.60 24.80-25:00-25.20-25.40— yd -m/z - 8 0705----- 13-.-4S%

5000 -65 77 106 i J 40 I I II I 120 132 I 159 170 rp-m-p- ' . ; j44+TpT-|Tpnprr|TTTT7+TTTpTWprTTTY^ L_ ............ / V......................... i,fe-> 30 40 50 60 jro 80 90 100 110 120 130 140 150 160 170 180 190 24.60 24.80 25.00 25.20 25.40

23838.D NP103001.M Thu Nov 01 14:33:36 2001 Page 4

NYC-WTC_000089356

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NYC-WTC_000089356Source: NYC Law Department, mirrored locally

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