GCMS calibration table for TCLP method, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : M:\INSTRU~l\209\DATA\DEC1301\29522.D Vial: 21 Acq On : 14 Dec 2001 4:25 am Operator: 209 GALOS Sample : gems scan 12/7 Inst : GC/MS 209 . Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title 209 625/TCLP calibration table Library C:\DATABASE\NBS75K.L

Peak Number 17 Nicodicodine Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

38.38 60.06 ug/1 17538800 Perylene-dl2 37.10

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Nicodicodine 406 C24H26N2O4 000808-24-2 18 2 2,3,9,10-Tetracyanodibenzo[5,5a,6:1 406 C24H6N8 000000-00-0 11 3 5-(4-Amyloxyphenyl)-2-(4-butoxy-2-h 406 C25H30N2O3 000000-00-0 10 4 2-(2-Hydroxy-4-nonyloxyphenyl)-5-(4 406 C25H30N2O3 000000-00-0 10 Abundance Scan 3631 (38.376 min): 29522.D (-) m/z 105.00 100.00% 105 391

5000

1 m/z-> 0- —Pr

Abundance 51 50 I 100I 125 149 178 —202— LL235—269 +-4--44 150 200 250 300 #54406: Nicodicodine 301 1327 360 350 400 447 450 "F ■ • i • * • ■ i ■ 38.00 38.20 38.40 38.60 38.80 m/z 391.15 83.19%

406

L _____ 5000 । 111 ■ ■ ■ ■ । ■ 38.00 38.20 38.40 38.60 38.80 284 m/z 406.20 52.98% 78 106 59 | T ' ' 198 226 248 1 1 350 m/z—> 50 100 150 200 250 300 350 400 450 Abundance #54403: 2,3,9.10-Tetracyanodibenzo[5.5a,6:11,11 a, 12]-1.4.7. 406 > "i yr 38.00 38.20 38.40 38.60 38.80 5000 m/z 392.15 25.72% 99 1 25 302 ; . 151 177198 224 250 275 328 354 380 I m/z-> 50 100 150 200 250 300 350 400 450 Abundance #54415: 5-(4-Amyioxyphenyl)-2-(4-butoxy-2-hydroxyphenyl)pyr TI TT 406 38.00 38.20 38.40 38.60 38.80 m/ z 00 21.95% 5000 280 350 118 89 | 223 251 3?2. 376 I I m/z-> 50 100 150 200 250 300 350 400 450 38.00 38.20 38.40 38.60 38.80

29522.D GCMS1126.M Tue Jan 08 10:55:14 2002 Page 17

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