GCMS sample AE12761 results, June 10 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File C:\MSDCHEM\1\DATA\060602\12762.D Vial: 8 Acq On 6 Jun 2002 5:00 pm Operator: McLean Sample 6/3 eh Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\060302.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 16 Isoquinolinium, 2-(m-nitroa... Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T. 34.86 0.89 ug/L 376492 Perylene-d12 34.65 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Isoquinolinium, 2-(m-nitroanilin... 265 C15H11N302 031383-03-6 28 2 Naphthalene, 1,2,3,4-tetrahydro-... 177 C10H11NO2 029809-14-1/22 3 Phosphine, dicyclohexylmethyl- 212 C13H25P 050420-46-7 17 4 Hydrazinecarboxamide, 2-(3-pheny... 189 C10H11N3O 003839-82-5 16 Abundance Scan 5408 (34.854 min): 12762.D (-5407) (-) m/z 129.50 '00.00% 129

117 5000 264 49

208 34.60 34.80 35.00 35.20

n/z-> O+ :20 o 40 60 FT ----- 80 100 120 140 160 180 200 220 240 260 281 280 m/z 130.50 72.66% Abundance #58359: Isoquinolinium, 2-(m-nitroanilino)-, hydroxide, in... 129

5000 65 102 ■ ' I ' - | Ilk 1. 34.60 34.80 35.00 35.20 50 90 265 m/Z 116.90 54.20% 219 — - Of t ■ ■ ■ ■ i ■ ■ ■ ■ i mfe-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #121949: Naphthalene, 1,2,3,4-tetrahydro-5-nitro- 130

115 159 MAA —H 34.60 34.80 35.00 35.20 5000 91 m/z 264.10 46.52% 32 77 51 65 103 177 Or Tr - I............................... 1 ‘ I ‘ ‘ ‘ I UCSITE J > | I J i : j I J i i j > » Wz-> 20 40 100 120 140 160 180 200 220 240 260 280 Abundance #58862: Phosphine, dicyclohexylmethyl- i i f i i i i |TT'>-r-| i i i i । i > 130 34.60 34.80 35.00 35.20 55 m/z 128.90 44.12% 41 50001 83 157 212 67 102115 197 29 । .'L .H Ji alll , |r | aldLL 1 +142 +rdh hsikpov 171183 I 0 ■ ' i ■ • ■ i ' ■ m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 34.60 34.80 35.00 35.20

12762.D 060302.M Mon Jun 10 10:26:56 2002 Page 19

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