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GCMS blank analysis for sample AE10303, May 2002

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Laboratory report showing blank analysis results for volatile organic compounds in sample AE10303 on May 9, 2002.

NYC-WTC_000045048–000045062

Folder label: “GCMS X 5/1/02 A 5/8/02

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NYC 9/11 Public Portal Document Library Search Compound Report Data File C:\MSDCHEM\1\DATA\050802\0501LB.D Vial: 3 Acq On 8 May 2002 3:26 pm Operator: Mclean Sample 5/1 eh Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\l\METHQDS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 6 3-(2-Methoxyphenyl)-1-methy... Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 34.91 0.42 ug/L 292468 Perylene-dl2 34.70

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-(2-Methoxyphenyl)-1-methyl-5-p. . . 265 C16H15N3O 1000210-16-8 9 2 Benzene, (1 hexyl-1-heptenyl)- 258 C19H30 055030-46-1 7/ 3 Isoquinolinium, 2-(p-nitroanilin... 265 C15H11N302 031383-05-8 /5 4 2H-Azepine-2-thione, hexahydro- 129 C6H11NS 007203-96-3 5 Abundance Scan 5417 (34.907 min): 0501 LB. D (-5416) (-) m/z 129.50 1003 00% 129

118 5000 207 258 281 40 96 231 7 S I 11 1 1 1 T77i 1‘‘7II‘I 34.60 34.80 35.00 35.20 0- 4 I I I i । । । 1 i | i 1 r TEr TT II m/z 118.10 63.52% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #52964: 3-(2-Methoxyphenyl)-1 -methyl-5-phenyl-1 H-[ 1,2,4]tr... 1 8 133 104 265 5000 77 91 236 i . । . . , - । > ri r-1 । । > । । । ! । । । 34.60 34.80 35.00 35.20 43 63 m/ z 128.80 50.27%! 147

m/z-> 0 44ulll-11 40100 —I 60 80 120 140 160 180 200 220 180 195297 222 I | । i ti । । r i । | >1 240 250 1 11 1 'T 260 279 280 Abundance #52900: Benzene, (1 hexyl-1 -heptenyl)- 1 8 1 1 1 11 1 1 rf 11 1 I 11 1 r i1 ’ 1 * i 34.60 34.80 35.00 35.20 5000 91 m/z 130.90 45.01%l 41 131 173 | 55 258 77 Til it 143 , 188 201213 228 o' 1 lpa 1 1 i„,.i ' 1 ----- 157 ■ ■ i ■ ■ ii । । r । ’। । । । ' । । • “I । । । । r

m/z->______ 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #58255: Isoquinolinium, 2-(p-nitroanilino)-, hydroxide, in... 1 ■ i 1 ■ 129 34.60 34.80 35.00 35.20 m/z 281.00 3 8.2 9%| 5000 63 102 75 235 265 51 ii i 90 , I, i l , , 165 190 218 O-r 1 1 1 1 1 1 ( 1 ‘ 11 T1 — 3 TI 1.11 1 I I ' I I "I I } I ■ < " I I I I | I I I I | ( I I j ! )1 11 ' ‘ ' i ' ■ ' ■ i Tl/z—> 40 60 80 100 120 140 160 180 200 220 240 260 280 34.60 34.80 35.00 35.20

0501LB.D 050102.M Thu May 09 13:47:15 2002 Page 9

NYC-WTC_000045060

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NYC-WTC_000045060Source: NYC Law Department, mirrored locally

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