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GCMS blank analysis for sample AE10303, May 2002

Machine-extracted title · confidence 100%

Laboratory report showing blank analysis results for volatile organic compounds in sample AE10303 on May 9, 2002.

NYC-WTC_000045048–000045062

Folder label: “GCMS X 5/1/02 A 5/8/02

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\050802\0501LB.D Vial: 3 Acq On 8 May 2002 3:26 pm Operator: Mclean Sample 5/1 eh Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title 508 Modified GC/MS scan Library C:\DATABASE\NIST98.L Peak Number 7 4-Pentenoic acid, 5-amino-3.. Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

34.97 0.42 ug/L 290310 Perylene-dl2 34.70

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 4-Pentenoic acid, 5-amino-3-oxo-.. 219 C12H13NO3 052812-85-8 9 2 Cyclopenta[cd]pentalene , 2a,4a,6.. 130 C10H10 006053-74-3 5 3 Benzene, 1-cyclobuten-l-yl - 130 C10H10 003365-26-2/5 4 Benzenamine, 2-(1-methylethenyl)- 133 C9H11N 052562-19-3 5 Abundance Scan 5427 (34.966 min): 0501 LB.D (-5426) (-) m/z 117.90 106.00% 73 1 8129

84 207 262 5000 44 7 _ I-1 I I I !—] I I I I I I > I I I I I I I I I

0 1 1 1 ' 1 i 1 1 ■ ■ i ........ ... I,! 34.60 34.80 35.00 35.20 m/ z 128.90 93.36% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #8295: 4-Pentenoic acid, 5-amino-3-oxo-5-phenyl-, methyl este 43 11 8

5000 59 84 146 1 । r 1 Myaa I A

34.60 34.80 35.00 35.20 103 219 159 m/z 73.10 83.39%

0! ■ ■ i 1 1 ' ' i ' 1 1 ' i' ........ I___________ . |

m/z—> 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #58454: Cyclopenta[cd]pentalene, 2a,4a,6a,6b-tetrahydro- . 115 129 1 5000 m/z 132.80 74.17%

20 51 64 77 39 II I il 189 103 O+ , 1 1 At dlrspmlyl, l.,- — /z-> 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #121839: Benzene, 1-cyclobuten-1-yl- 129 34.60 34.80 35.00 35.20 115 m/ z 13 0.60 61.62% 102 5000 51 77 39 63 91 _ 1 , il II I , .1 0 ' 1 ( 1 ' 1 1 1 1 ' 1 1 I • ' ' ' ] I— TIT । । । i i i । । । । । । । । 1 । t । m । । । । > cn । । । । । । । i 1 ' i ' ■ ' i 1 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 34.60 34.80 35.00 35.20

0501LB.D 050102.M Thu May 09 13:47:16 2002 Page 10

NYC-WTC_000045061

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NYC-WTC_000045061Source: NYC Law Department, mirrored locally

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