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GCMS calibration table for TCLP method, Dec 2001

Machine-extracted title · confidence 100%

Quality reviewed GCMS calibration data listing surrogate compounds and retention times from December 14, 2001.

NYC-WTC_000036729–000036751

Folder label: “GCMS X 12/7/01 A 1/2/02

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Scanned page image, NYC-WTC_000036751
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NYC 9/11 Public Portal Document

Tentatively Identified Compound (LSC) summary

Operator ID: 209 GALOS Date Acquired: 14 Dec 2001 4:25 am Data File: M:\INSTRU~1\209\DATA\DEC1301\29522.D Name: gems scan 12/7 Mise: Method: C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title: 209 625/TCLP calibration table Library Searched: C:\DATABASE\NBS75K.L

TIC Top Hit name RT EstConc Units Area IntStd ISRT ISArea ISConc

N=Ethylformami de 7.59 2.5 ug/1 922644 ISTD01 11.67 7467030 20.0 Platinum, bis [(1,2,5 11.84 12.1 ug/1 4525060 ISTD01 11.67 7467030 20.0 Carbamothioic acid, 16.52 1.8 ug/1 844994 ISTD02 15.28 9492640 20.0 Propanenitrile, 3,3' 18.19 1.1 ug/1 539198 ISTD03 20.56 10261700 20.0 Benzene methoxybi s ( 21.65 2.1 ug/1 1081830 ISTD03 20.56 10261700 20.0 1H—Pyrazole, 4,5-dih 22.93 2.3 ug/1 1120690 ISTD04 24.98 9905290 20.0 Benzoic acid, thio-, 23.10 49.7 ug/1 24608000 ISTD04 24.98 9905290 20.0 Naphthalene , 1,6-dim 24.00 15.4 ug/1 7647250 ISTD04 24.98 9905290 20.0 Phenol, 3,5-bis (1,1- 24.36 2.4 ug/1 1191750 ISTD04 24.98 9905290 20.0 Permethrin 25.12 8.9 ug/1 4401420 ISTD04 24.98 9905290 20.0 Pyrazin, tetramethy 25.30 1.0 ug/1 515100 ISTD04 24.98 9905290 20.0 E thy142 a c e t y l b e n z o a 32.20 22.1 ug/1 34682300 ISTD05 33.02 31324600 20.0 2H-Pyran-2-one, 6-[2 32.24 5.7 ug/1 8969950 ISTD05 33.02 31324600 20.0 Phosphonic acid, phe 32.41 6.3 ug/1 9815970 ISTD05 33.02 31324600 20.0 Decanedioic acid, bi 35.57 6.2 ug/1 1815270 ISTD06 37.10 5840890 20.0 Nicedicodi ne 38.18 64.3 ug/1 18777400 ISTD06 37.10 5840890 20.0 Ni icodine 38.38 60.1 ug/1 17538800 ISTD06 37.10 5840890 20.0

29522 .D GCMS1126.M Tue Jan 08 10:55:14 2002

NYC-WTC_000036751

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NYC-WTC_000036751Source: NYC Law Department, mirrored locally

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