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GCMS analysis results for sample AD29563, Jan 2002

Machine-extracted title · confidence 100%

GCMS analysis report for sample AD29563 listing unknown compounds and surrogate recovery data from January 28, 2002.

NYC-WTC_000036712–000036728

Folder label: “GCMS X 12/7/01 A 1/2/02

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Scanned page image, NYC-WTC_000036717
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NYC 9/11 Public Portal Document

LSC Area Percent Report

• Data. File : C:\HPCHEM\l\DATA\DEC2701\29563.D Vial 36 Acq On : 28 Dec 2001 11:11 pm Operator 209 GALOS Sample : GC/MS SCAN 12/7 Inst GC/MS 209 Mise : Multiplr 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.612 276 280 311 rBV 349244 1278561 11.65% 2.105% 2 11.128 658 663 675 rBV 127623 352887 3.22% 0.581% 3 11.678 717 723 749 rBV 2744334 8455865 77.06% 13.918% 4 14.304 1000 1009 1016 rBV 406814 895660 8.16% 1.474% 5 15.277 1110 1115 1134 rBV 4168373 10394852 94.73% 17.110%

6 17.453 1345 1352 1362 rBV 641052 1351962 12.32% 2.225% 7 20.271 1653 1659 1668 rBV 440947 937892 8.55% 1.544% 8 20.. 565 1684 1691 1707 rBV 4695445 10973187 100.00% 18.062% 9 21.042 1738 1743 1763 rBV 65905 310776 2.83% 0.512% 10 22.787 1927 1933 1940 rBV 272705 583903 5.32% 0.961%

11 24.981 2163 2172 2186 rBV2 4045166 10645579 97.01% 17.523% 12 26.890 2373 2380 2388 rBV 126538 264019 2.41% 0.435% 13 28.653 2563 2572 2578 rBV 88019 197816 1.80% 0.326% 14 30.057 2720 2725 2735 rBV 466509 1065362 9.71% 1.754% 15 30.250 2740 2746 2753 rVB 71227 166574 1.52% 0.274%

16 31.719 2900 2906 2913 rBV 55028 141249 1.29% 0.232% 17 33.023 3041 3048 3072 rBV2 2793661 7565494 68.95% 12.453% 18 37.117 3486 3494 3520 rBV2 1598286 5171128 47.13% 8.512%

Sum of corrected areas: 60752766

29563.D GCMS1126.M Tue Jan 08 11:41:51 2002

NYC-WTC_000036717

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NYC-WTC_000036717Source: NYC Law Department, mirrored locally

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