GCMS analysis comments for sample AD28678, Dec 2001

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LSC Area Percent Report Data File : C:\HPCHEM\l\DATA\DEC0401\28678.D Vial: 16 Acq On : 5 Dec 2001 3:01 am Operator 209 GALOS Sample : gc/ms 11/24 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.796 296 300 319 rVB 15373 63895 1.06% 0.202% 2 11.716 721 727 747 rBV 1622846 4513420 74.98% 14.256% 3 15.314 1113 1119 1137 rBV 2797152 5858098 97.32% 18.503% 4 20.584 1687 1693 1712 rBV 2763272 6019240 100.00% 19.012% 5 25.009 2168 2175 2187 rBV2 2396087 5381914 89.41% 16.999%

6 29.434 2649 2657 2665 rBV 455787 897511 14.91% 2.835% 7 29.553 2665 2670 2676 rW 89126 187690 3.12% 0.593% 8 29.682 2679 2684 2694 rVB 72943 154706 2.57% 0.489% 9 30.076 2722 2727 2735 rVB 205803 406673 6.76% 1.284% 10 30.627 2781 2787 2796 rBV 35920 175698 2.92% 0.555%

11 31.573 2885 2890 2896 rBV 248936 504766 8.39% 1.594'% 12 31.664 2896 2900 2908 rW 131384 284971 4.73% 0.900% 13 32.656 3002 3008 3020 rBV 94154 206783 3 .44% 0.653% 14 33.032 3043 3049 3070 rBV2 1544493 3731722 62.00% 11.787% 15 33.611 3107 3112 3121 rBV 93140 219189 3.64% 0.692%

16 34.538 3208 3213 3222 rBV 58658 129555 2.15% 0.409% 17 35.428 3304 3310 3320 rBV 40655 106142 1.76% 0.335% 18 37.127 3488 3495 3513 rBV2 991706 2818270 46.82% 8.902%

Sum of corrected areas: 31660243

28678.D GCMS1126.M Thu Dec 06 15:13:27 2001

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