GCMS analysis comments for sample AD28694, Dec 2001

NYC 9/11 Public Portal Document

LSC Area Percent Report Data File : C:\HPCHEM\1\DATA\DEC0401\28694.D Vial: 5 Acq On : 4 Dec 2001 4:16 pm Operator: 209 GALOS Sample : gc/ms 11/24 Inst : GC/MS 209 Mise 2 Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 11.716 721 727 747 rBV 1978711 5097329 72.92% 12.938% 2 15.314 1113 1119 1137 rBV 3100084 6611498 94.58% 16.781% 3 20.584 1687 1693 1717 rBV 3160365 6990289 100.00% 17.743% 4 25.009 2168 2175 2187 rBV2 2969285 6505927 93.07% 16.513% 5 25.156 2187 2191 2197 rVB 28619 84642 1.21% 0.215%

6 27.010 2390 2393 2398 rBV 43664 83685 1.20% 0.212% 7 29.434 2652 2657 2666 rBV 510029 1020767 14.60% 2.591% 8 29.553 2666 2670 2676 rW 59774 124756 1.78% 0.317% 9 29.682 2680 2684 2695 rVB 73820 149937 2.14% 0.381% 10 30.076 2722 2727 2733 rBV 422761 873084 12.49% 2.216%

11 30.627 2782 2787 2796 rBV 64595 128225 1.83% 0.325% 12 31.573 2884 2890 2896 rBV2 309161 641444 9.18% 1.628% 13 31.665 2896 2900 2910 rW 90429 206357 2.95% 0.524% 14 32.656 3003 3008 3015 rBV 66162 144607 2.07% 0.367% 15 33.042 3043 3050 3063 rBV2 2054867 4939452 70.66% 12.537%

16 33.611 3105 3112 3120 rBV 71221 173378 2.48% 0.440% 17 34.538 3207 3213 3220 rBV2 42271 106550 1.52% 0.270% 18 35.428 3305 3310 3320 rBV 31135 82976 1.19% 0.211% 19 35.594 3322 3328 3349 rBV 474335 1341919 19.20% 3.406% 20 37.136 3487 3496 3514 rBV2 1422913 4091152 58.53% 10.384%

Sum of corrected areas: 39397974

28694.D GCMS1126.M Thu Dec 06 15:33:51 2001

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