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GCMS analysis results for sample AD30425, Jan 2002

Machine-extracted title · confidence 95%

Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30425 conducted on January 10, 2002.

NYC-WTC_000017703–000017723

Folder label: “GCMS X 12/13/01 A 12/27/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\1\DATA\DEC2701\30425.D Vial: 5 Acq On : 27 Dec 2001 3:04 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/13 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF’ Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 6.392 144 147 157 rBV 30249 87766 1.03% 0.177% 2 7.613 276 280 314 rVB 548636 1537743 18.08% 3.100% 3 11.129 659 663 672 rBV 71807 169767 2.00% 0.342% 4 11.358 684 688 693 rBV 38381 99386 1.17% 0.200% 5 11.441 693 697 711 rVB 42221 158868 1.87% 0.320%

6 11.679 718 723 741 rBV 2416953 6138631 72.19% 12.375% 7 14.305 1003 1009 1017 rBV 424167 875272 10.29% 1.765% 8 15.278 1110 1115 1135 rBV 3162799 7582322 89.17% 15.286% 9 17.454 1345 1352 1360 rBV2 708655 1478710 17.39% 2.981%' 10 20.272 1653 1659 1666 rBV 567683 1172955 13.79% 2.365%

11 20.557 1684 1690 1716 rBV 3641439 8503227 100.00% 17.142% 12 22.788 1927 1933 1942 rBV 426713 888955 10.45% 1.792% 13 24.982 2163 2172 2187 rBV2 3119955 8435231 99.20% 17.005% 14 26.891 2371 2380 2386 rBV 245199 523148 6.15% 1.055% 15 27.010 2387 2393 2405 rVB 46469 129130 1.52% 0.260%

16 28.654 2562 2572 2582 rBV 187356 419017 4.93% 0.845% 17 30.058 2719 2725 2735 rBV 594353 1309001 15.39% 2.639% 18 30.251 2740 2746 2755 rVB 140723 340744 4.01% 0.687% 19 31.720 2900 2906 2916 rVB 95217 267334 3.14% 0.539% 20 33.024 3041 3048 3070 rBV 2066435 5608410 65.96% 11.306%

21 34.373 3189 3195 3208 rBV 40061 145818 1.71% 0.294% 22 35.567 3318 3325 3335 rBV3 22669 90153 1.06% 0.182% 23 37.118 3486 3494 3517 rBV2 1101176 3642285 42.83% 7.343%

Sum of corrected areas: 49603873

30425.D GCMS1126.M Wed Jan 02 11:03:26 2002

NYC-WTC_000017708

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NYC-WTC_000017708Source: NYC Law Department, mirrored locally

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