GCMS analysis comments for sample AD28691, Dec 2001

NYC 9/11 Public Portal Document

LSC Area Percent Report Data File : C: \HPCHEM\1\DATA\DEC0401\28691.D vial: 11 Acq On 4 Dec 2001 10:08 pm Operator: 209 GALOS Sample : gc/ms 11/24 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 7.661 281 285 293 rBV 36234 95862 1.48% 0.249% 2 11.709 721 726 746 rBV 1873767 4560118 70.52% 11.866% 3 15.317 1113 1119 1136 rBV 2816938 6031544 93.28% 15.695% 4 20.587 1686 1693 1714 rBV 2978610 6466119 100.00% 16.826% 5 25.003 2168 2174 2186 rBV2 2651410 5898533 91.22% 15.349% 6 25.149 2187 2190 2199 rVB 23688 73890 1.14% 0.192% 7 29.437 2652 2657 2665 rBV 1072683 2123227 32.84% 5.525% 8 29.556 2665 2670 2678 rW 120725 265911 4.11% 0.692% 9 29.684 2678 2684 2697 rVB 124813 270660 4.19% 0.704% 10 30.079 2721 2727 2738 rBV 338844 691385 10.69% 1.799% 11 30.630 2782 2787 2794 rBV 129900 253767 3.92% 0.660% 12 31.576 2883 2890 2896 rBV 683911 1492883 23.09% 3.885% 13 31.667 2896 2900 2910 rW 190377 441012 6.82% 1.148% 14 31.796 2910 2914 2925 rVB2 41101 107718 1.67% 0.280% 15 32.659 3002 3008 3015 rBV 153691 325553 5.03% 0.847% 16 33.035 3042 3049 3068 rBV2 1915108 4558131 70.49% 11.861% 17 33.614 3102 3112 3124 rBV 165932 387370 5.99% 1.008% 18 34.532 3207 3212 3223 rBV 97814 247833 3.83% 0.645% 19 35.422 3303 3309 3320 rBV 77517 212422 3.29% 0.553% 20 36.285 3397 3403 3412 rBV2 38899 115981 1.79% 0.302% 21 37.130 3487 3495 3520 rBV2 1301923 3810046 58.92% 9.914%

Sum of corrected areas: 38429965 28691.D GCMS1126.M Thu Dec 06 13:26:24 2001

NYC-WTC_000035056