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GCMS analysis results for sample AD28471, Dec 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD28471 conducted on December 6, 2001.

NYC-WTC_000034347–000034365

Folder label: “GCMS X 11/21/01 A 11/27 - 11/28/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\HPCHEM\1\DATA\DEC0401\28471.D Vial: 7 Acq On 4 Dec 2001 6:13 pm Operator: 209 GALOS Sample gc/ms 11/24 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak peak peak % Of # min scan scan scan TY height area % max. total

1 11.711 721 726 744 rBV 2194911 5258925 72.51% 12.507% 2 15.319 1113 1119 1136 rBV 3159539 6932210 95.58% 16.487% 3 20.588 1686 1693 1710 rBV 3283845 7252497 100.00% 17.249% 4 25.004 2168 2174 2186 rBV2 3001299 6754516 93.13% 16.064% 5 25.151 2186 2190 2198 rVB 29818 88724 1.22% 0.211%

6 29.438 2651 2657 2665 rBV 965647 . 1902672 26.23% 4.525% 7 29.548 2665 2669 2675 rW 111551 241390 3.33% 0.574% 8 29.686 2679 2684 2696 rVB 106299 234827 3.24% 0.558% 9 30.081 2721 2727 2735 rBV 357112 748686 10.32% 1.781% 10 30.632 2781 2787 2794 rBV 114276 232880 3.21% 0.554%

11 31.568 2883 2889 2895 rBV 558834 1198560 16.53% 2.851% 12 31.660 2895 2899 2909 rW 173942 396316 5.46% 0.943% 13 31.797 2909 2914 2922 rVB2 34348 85139 1.17% 0.202% 14 32.660 3002 3008 3015 rBV 131466 286354 3.95% 0.681% 15 33.037 3039 3049 3068 rBV2 2218524 5255371 72.46% 12.499%

16 33.615 3104 3112 3122 rBV 141432 331071 4.56% 0.787% 17 34.533 3206 3212 3221 rBV 92692 221653 3.06% 0.527% 18 35.424 3304 3309 3323 rBV 72096 193941 2.67% 0.461% 19 36.287 3398 3403 3409 rBV 33925 89722 1.24% 0.213% 20 37.131 3487 3495 3516 rBV2 1484484 4341563 59.86% 10.325%

Sum of corrected areas: 42047017

28471.D GCMS1126.M Wed Dec 05 11:27:22 2001

NYC-WTC_000034352

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NYC-WTC_000034352Source: NYC Law Department, mirrored locally

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