GCMS analysis comments for sample AD28663, Dec 2001

NYC 9/11 Public Portal Document LSC Area Percent Report . Data File C: \HPCHEM\ 1 \DATA\DECO 4 01\28663.D Vial: 17 Acq On 5 Dec 2001 3:59 am Operator: 209 GALOS Sample gc/ms 11/24 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 11.715 721 727 745 rBV 1666804 4478442 74.46% 13.392% 2 15.314 1113 1119 1138 rBV 2727075 5782522 96.15% 17.291% 3 20.583 1687 1693 1710 rBV 2721913 6014332 100.00% 17.985% 4 25.008 2168 2175 2187 rBV2 2524296 5522745 91.83% 16.515% 5 25.155 2187 2191 2199 rVB 20221 65216 1.08% 0.195%

6 29.442 2651 2658 2665 rBV 600614 1238831 20.60% 3.704% 7 29.552 2665 2670 2676 rW 100672 206427 3 .43% 0.617% 8 29.681 2679 2684 2694 rW 84120 186953 3.11% 0.559% 9 30.076 2722 2727 2740 rBV 347047 701031 11.66% 2.096% 10 30.626 2781 2787 2799 rBV 94524 195521 3.25% 0.585%

11 31.572 2883 2890 2896 rBV 360405 735609 12.23% 2.200% 12 31.664 2896 2900 2910 rW 146359 327375 5.44% 0.979% 13 31.801 2910 2915 2922 rVB2 26128 64697 1.08% 0.193% 14 32.655 3002 3008 3017 rBV 103082 231745 3.85% 0.693% 15 33.032 3042 3049 3064 rBV2 1627264 3971948 66.04% 11.877%

16 33.610 3104 3112 3123 rBV 107920 259425 4.31% 0.776% 17 34.537 3207 3213 3221 rBV 70110 167738 2.79% 0.502% 18 35.428 3304 3310 3316 rBV 49537 128905 2.14% 0.385% 19 36.281 3398 3403 3414 rBV2 23323 63591 1.06% 0.190% 20 37.126 3488 3495 3515 rBV2 1070047 3098597 51.52% 9.266%

Sum of corrected areas: 33441650

28663.D GCMS1126.M Thu Dec 06 15:31:16 2001

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