GCMS analysis comments for sample AD28664, Dec 2001

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LSC Area Percent Report

Data File C:\HPCHEM\l\DATA\DEC0401\28664.D Vial: 18 Acq On 5 Dec 2001 4:58 am Operator: 209 GALOS Sample gc/ms 11/24 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 11.707 721 726 748 rBV 1833720 5067578 74.59% 13.865% 2 15.315 1113 1119 1138 rBV 3093442 6565833 96.64% 17.964% 3 20.584 1687 1693 1716 rBV 3041749 6793918 100.00% 18.588% 4 25.009 2168 2175 2187 rBV2 2842779 6262542 92.18% 17.134% 5 25.147 2187 2190 2201 rVB2 24962 77223 1.14% 0.211%

6 29.434 2652 2657 2666 rBV 536970 1087563 16.01% 2.976% 7 29.554 2666 2670 2676 rW 68213 137551 2.02% 0.376% 8 29.682 2679 2684 2693 rW 69782 151351 2.23% 0.414% 9 30.077 2722 2727 2733 rBV 360027 709317 10.44% 1.941%, 10 30.628 2783 2787 2795 rVB 61617 123275 1.81% 0.337%

11 31.573 2883 2890 2896 rBV 350974 710239 10.45% 1.943% 12 31.665 2896 2900 2910 rW 101431 228093 3.36% 0.624% 13 32.657 3003 3008 3015 rBV 69691 151784 2.23% 0.415% 14 33.042 3042 3050 3069 rBV2 1855597 4577770 67.38% 12.525% 15 33.611 3106 3112 3119 rBV 68521 168205 2.48% 0.460%

16 34.538 3207 3213 3219 rBV 43913 101500 1.49% 0.278% 17 35.429 3304 3310 3316 rBV2 30206 80769 1.19% 0.221% 18 37.127 3488 3495 3517 rBV2 1222933 3555653 52.34% 9.728%

Sum of corrected areas: 36550164

28664.D GCMS1126.M Fri Dec 07 15:53:24 2001

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