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GCMS blank analysis for sample AD28662, Dec 2001

Machine-extracted title · confidence 100%

Blank test results confirming no detectable contaminants above method detection limits for sample AD28662.

NYC-WTC_000034971–000034987

Folder label: “GCMS X 11/24/01 A 12/4/01

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NYC 9/11 Public Portal Document LSC Area Percent Report Data File : C:\HPCHEM\l\DATA\DEC0401\28662.D Vial: 15 Acq On : 5 Dec 2001 2:02 am Operator : 209 GALOS Sample : gc/ms 11/24 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs : 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 11.709 721 726 745 rBV 1859545 4648112 74.02% 13.803% 2 15.317 1113 1119 1137 rBV 2827059 6058566 96.47% 17.992% 3 20.586 1687 1693 1716 rBV 2881741 6279953 100.00% 18.649% 4 25.002 2168 2174 2187 rBV2 2530261 5726475 91.19% 17.006% 5 25.149 2187 2190 2202 rVB2 19941 71305 1.14% 0.212% 6 29.436 2652 2657 2665 rBV 542169 1028179 16.37% 3.053% 7 29.546 2665 2669 2679 rVB 58798 126168 2.01% 0.375% 8 29.684 2679 2684 2692 rBV2 53725 115855 1.84% 0.344% 9 30.079 2722 2727 2736 rBV 320710 619769 9.87% 1.841% 10 30.630 2781 2787 2798 rBV 56467 110778 1.76% 0.329% 11 31.575 2884 2890 2896 rBV 294882 610823 9.73% 1.814% 12 31.667 2896 2900 2910 rW 87782 201340 3.21% 0.598% 13 32.658 3001 3008 3015 rBV 61537 130731 2.08% 0.388% 14 33.035 3042 3049 3070 rBV2 1835276 4304884 68.55% 12.784% 15 33.613 3106 3112 3123 rVB 66144 144615 2.30% 0.429% 16 34.540 3206 3213 3220 rBV 36245 90127 1.44% 0.268% 17 35.422 3301 3309 3318 rBV 27483 69644 1.11% 0.207% 18 37.129 3486 3495 3519 rBV2 1166810 3336461 53.13% 9.908%

Sum of corrected areas: 33673785 28662.D GCMS1126.M Thu Dec 06 13:19:55 2001

NYC-WTC_000034975

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NYC-WTC_000034975Source: NYC Law Department, mirrored locally

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