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GCMS analysis results for sample AD30351, Jan 2002

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Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30351 conducted on January 10, 2002.

NYC-WTC_000017833–000017853

Folder label: “GCMS X 12/13/01 A 12/27/01

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NYC 9/11 Public Portal Document LSC Area Percent Report

• Data File : C:\HPCHEM\l\DATA\DEC2701\30351.D Vial: 20 Acq On : 28 Dec 2001 6:36 am Operator: 209 GALOS Sample : GC/MS SCAN 12/13 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.613 276 280 293 rBV 448096 1153038 14.10% 2.406% 2 11.129 658 663 676 rBV 81143 196289 2.40% 0.410% 3 11.671 718 722 750 rBV 2121997 5650748 69.10% 11.789% 4 14.306 1002 1009 1020 rBV 433328 907962 11.10% 1.894% 5 15.279 1109 1115 1134 rBV 2942631 7013138 85.76% 14.631%

6 17.455 1345 1352 1361 rBV 796609 1711856 20.93% 3.571% 7 20.273 1653 1659 1666 rBV 700662 1452488 17.76% 3.030% 8 20.558 1684 1690 1715 rBV 3339879 7807131 95.47% 16.288% 9 22.788 1927 1933 1944 rBV 563399 1170797 14.32% 2.443% 10 24.982 2163 2172 2215 rBV3 2779405 8177875 100.00% 17.061% 11 26.892 2374 2380 2388 rBV 333755 713649 8.73% 1.489% 12 27.011 2388 2393 2403 rW 45335 130299 1.59% 0.272% 13 28.655 2564 2572 2580 rBV 264346 588013 7.19% 1.227% 14 30.059 2720 2725 2739 rBV 530889 1150675 14.07% 2.401% 15 30.252 2739 2746 2756 rW 225043 535604 6.55% 1.117%

16 31.712 2895 2905 2917 rBV 175338 472226 5.77% 0.985% 17 33.024 3041 3048 3053 rBV2 1891012 4876531 59.63% 10.174% 18 34.374 3188 3195 3207 rBV 90599 308833 3.78% 0.644% 19 35.567 3318 3325 3340 rBV 61171 244275 2.99% 0.510% 20 36.715 3444 3450 3455 rBV2 26420 86792 1.06% 0.181% 21 37.119 3486 3494 3521 rBV 1066324 3584143 43.83% 7.478%

Sum of corrected areas: 47932362

30351.D GCMS1126.M Wed Jan 02 10:45:43 2002

NYC-WTC_000017838

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NYC-WTC_000017838Source: NYC Law Department, mirrored locally

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