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Document / 344 pages

DEP GCMS data table, Jan-Feb 2002

Machine-extracted title · confidence 90%

Large multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

NYC-WTC_000004149–000004492

Folder label: “GCMS X 12/18/01, 2/8/02 A 2/10/02, 1/10/02, 1/14/02

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Scanned page image, NYC-WTC_000004338
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NYC 9/11 Public Portal Document

LSC Area Percent Report

■ Data File : C:\HPCHEM\1\DATA\DEC2 701\30708.D Vial: 49 Acq On : 30 Dec 2001 6:21 am Operator: 209 GALOS Sample : GC/MS SCAN 12/18 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.617 276 280 294 rBV 454672 1244792 9.54% 1.608% 2 7.764 294 296 309 rVB2 37452 135253 1.04% 0.175% 3 11.133 657 663 674 rBV 185139 456298 3.50% 0.589% 4 11.674 717 722 746 rBV 3669493 9266735 71.05% 11.970% 5 14.309 999 1009 1016 rBV 952629 2032052 15.58% 2.625%

6 15.282 1109 1115 1134 rBV 4937794 11607898 89.00% 14.994% 7 17.449 1344 1351 1361 rBV2 1598678 3501503 26.85% 4.523% 8 18.156 1423 1428 1434 rBV 81705 168085 1.29% 0.217% 9 20.276 1653 1659 1670 rBV 1232294 2634035 20.19% 3.402% 10 20.561 1683 1690 1706 rBV 5366793 12340201 94.61% 15.940%'

11 21.029 1737 1741 1759 rBV 194199 663338 5.09% 0.857% 12 22.792 1926 1933 1944 rBV 792562 1726826 13.24% 2.231% 13 24.986 2159 2172 2186 rBV2 4810502 13043193 100.00% 16.848% 14 26.886 2373 2379 2386 rBV 410989 867757 6.65% 1.121% 15 28.649 2565 2571 2580 rBV 307955 685348 5.25% 0.885%

16 30.063 2718 2725 2733 rBV 480909 1044932 8.01% 1.350% 17 30.246 2739 2745 2753 rBV 271646 612096 4.69% 0.791% 18 31.715 2899 2905 2917 rVB 231052 547494 4.20% 0.707% 19 33.028 3040 3048 3053 rBV2 3335372 8363244 64.12% 10.803% 20 34.368 3188 3194 3207 rBV 129045 360755 2.77% 0.466%

21 35.571 3317 3325 3337 rBV 136242 421995 3.24% 0.545% 22 36.709 3443 3449 3460 rBV2 43842 139820 1.07% 0.181% 23 37.122 3486 3494 3526 rBV2 1735171 5553869 42.58% 7.174%

Sum of corrected areas: 77417519

30708.D GCMS1126.M Mon Jan 28 11:28:03 2002

NYC-WTC_000004338

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NYC-WTC_000004338Source: NYC Law Department, mirrored locally

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