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GCMS calibration table for TCLP analysis, Nov 2001

Machine-extracted title · confidence 100%

Calibration data sheet recording response factors and retention times for standard compounds used in GCMS TCLP analysis on November 26-27, 2001.

NYC-WTC_000033911–000033935

Folder label: “GCMS X 11/20/01 A 11/26/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

' Data File : C:\HPCHEM\1\DATA\JAN0802\28327.D Vial: 5 Acq On : 8 Jan 2002 4:16 pm Operator: 209 GALOS Sample : 508 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 11.391 687 691 700 rBV 71358 186325 1.67% 0.256% 2 11.529 700 706 718 rW 2643773 7182772 64.50% 9.866% 3 14.164 988 993 1000 rVB 523496 1064211 9.56% 1.462% 4 15.128 1092 1098 1116 rBV 4304172 9364448 84.10% 12.863% 5 17.303 1327 1335 1344 rBV 2019346 4344877 39.02% 5.968%

6 18.001 1406 1411 1417 rBV 257867 476234 4.28% 0.654% 7 20.122 1637 1642 1650 rW 1879226 4068414 36.54% 5.588% 8 20.397 1665 1672 1686 rBV 4623509 9975641 89.59% 13.703% 9 20.571 1687 1691 1696 rVB 127651 234380 2.10% 0.322% 10 20.847 1716 1721 1726 rBV 892675 1712471 15.38% 2.352%'

11 22.637 1910 1916 1929 rBV 1404973 2929167 26.31% 4.023% 12 24.813 2146 2153 2165 rBV3 4802748 11135385 100.00% 15.296% 13 26.731 2355 2362 2369 rBV 744127 1594835 14.32% 2.191% 14 28.503 2548 2555 2563 rBV 574698 1299813 11.67% 1.785% 15 29.880 2699 2705 2714 rBV 498794 1026918 9.22% 1.411%

16 30.091 2722 2728 2743 rVB 491875 1153682 10.36% 1.585% 17 31.560 2882 2888 2901 rBV 414337 1015718 9.12% 1.395% 18 32.846 3020 3028 3033 rBV2 2825489 6723053 60.38% 9.235% 19 32.937 3033 3038 3055 rVB 336105 1015959 9.12% 1.396% 20 34.223 3171 3178 3197 rBV 198064 705173 6.33% 0.969%

21 35.425 3301 3309 3324 rBV 113224 453817 4.08% 0.623% 22 36.554 3425 3432 3448 rBV 63238 262151 2.35% 0.360% 23 36.912 3461 3471 3486 rBV2 1723304 4738378 42.55% 6.509% 24 37.821 3559 3570 3578 rBV 31350 137729 1.24% 0.189%

Sum of corrected areas: 72801551

28327.D GCMS1126.M Wed Jan 09 09:14:27 2002

NYC-WTC_000033916

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NYC-WTC_000033916Source: NYC Law Department, mirrored locally

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