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Document / 344 pages

DEP GCMS data table, Jan-Feb 2002

Machine-extracted title · confidence 90%

Large multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

NYC-WTC_000004149–000004492

Folder label: “GCMS X 12/18/01, 2/8/02 A 2/10/02, 1/10/02, 1/14/02

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Scanned page image, NYC-WTC_000004441
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NYC 9/11 Public Portal Document

LSC Area Percent Report

' Data File : C:\HPCHEM\l\DATA\DEC2701\30707.D Vial: 41 Acq On : 29 Dec 2001 10:35 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/18 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.609 275 279 292 rBV 359214 1090486 8.50% 1.342% 2 11.134 657 663 674 rBV 70776 199646 1.56% 0.246% 3 11.675 717 722 750 rVB 3179470 8677998 67.63% 10.679% 4 14.310 999 1009 1017 rBV 953198 2102743 16.39% 2.587% 5 15.283 1109 1115 1133 rBV 4592494 10968381 85.48% 13.497%

6 17.450 1342 1351 1360 rBV 2239742 4933583 38.45% 6.071% 7 18.157 1422 1428 1434 rBV 198099 399288 3.11% 0.491% 8 20.277 1652 1659 1669 rBV 1758635 3916548 30.52% 4.819% 9 20.562 1683 1690 1706 rBV2 5119154 11675736 91.00% 14.367% 10 21.030 1736 1741 1761 rVB 183003 675661 5.27% 0.831%

11 22.793 1926 1933 1946 rBV 1141027 2599332 20.26% 3.199% 12 24.987 2162 2172 2185 rBV3 4445962 12830884 100.00% 15.789% 13 26.887 2373 2379 2387 rBV 622284 1342347 10.46% 1.652% 14 28.650 2565 2571 2580 rVB 474547 1078874 8.41% 1.328% 15 30.064 2719 2725 2736 rBV 449899 1008652 7.86% 1.241%

16 30.247 2739 2745 2757 rVB 425587 984004 7.67% 1.211% 17 31.716 2899 2905 2916 rBV 361925 880338 6.86% 1.083% 18 33.029 3040 3048 3052 rBV2 3144664 7869667 61.33% 9.684% 19 33.084 3052 3054 3070 rVB 405204 1083683 8.45% 1.334% 20 34.369 3188 3194 3212 rBV 211565 654393 5.10% 0.805%

21 35.572 3319 3325 3338 rBV 153544 504016 3.93% 0.620% 22 36.719 3443 3450 3462 rBV2 75365 273382 2.13% 0.336% 23 37.123 3485 3494 3518 rBV2 1669848 5364740 41.81% 6.601% 24 38.023 3585 3592 3603 rBV2 36671 151231 1.18% 0.186%

Sum of corrected areas: 81265613

30707.D GCMS1126.M Mon Jan 28 11:23:29 2002

NYC-WTC_000004441

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NYC-WTC_000004441Source: NYC Law Department, mirrored locally

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