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GC/MS calibration data for sample 30643, Dec 2001

Machine-extracted title · confidence 100%

Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.

NYC-WTC_000018445–000018469

Folder label: “GCMS X 12/18/01 A 12/30/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\1\DATA\DEC2701\30643.D Vial: 59 Acq On : 30 Dec 2001 5:02 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/18 A Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % Of # min scan scan scan TY height area % max. total

1 7.614 276 280 292 rBV 529817 1384936 9.42% 1.400% 2 7.752 293 295 314 rVB2 46498 178693 1.22% 0.181% 3 11.130 657 663 676 rBV 586079 1402063 9.53% 1.418% 4 11.672 717 722 747 rBV 3896117 9896699 67.30% 10.007% 5 14.306 999 1009 1017 rBV 1931895 4179623 28.42% 4.226%

6 15.279 1109 1115 1134 rBV 5346219 12254073 83.33% 12.391% 7 17.455 1343 1352 1362 rBV 2934947 6637332 45.14% 6.711% 8 18.153 1422 1428 1434 rBV 149144 308603 2.10% 0.312% 9 20.274 1652 1659 1668 rBV 2245429 5080958 34.55% 5.138% 10 20.558 1683 1690 1707 rBV 5502349 13199440 89.76% 13.347%

11 21.026 1734 1741 1762 rBV 242574 843754 5.74% 0.853% 12 22.789 1927 1933 1946 rBV 1593463 3453543 23.49% 3.492% 13 24.983 2162 2172 2186 rBV3 5015990 14705152 100.00% 14.869% 14 26.883 2373 2379 2387 rBV 791362 1801083 12.25% 1.821% 15 28.655 2566 2572 2583 rBB 646544 1456783 9.91% 1.473%

16 30.060 2719 2725 2737 rBV 564153 1223556 8.32% 1.237% 17 30.243 2739 2745 2756 rVB 571063 1359015 9.24% 1.374% 18 31.712 2898 2905 2920 rBV 520053 1224180 8.32% 1.238% 19 33.025 3041 3048 3053 rBV2 3557029 8960362 60.93% 9.060% 20 33.080 3053 3054 3073 rVB 546922 1250086 8.50% 1.264%

21 34.374 3188 3195 3209 rBV 315955 901127 6.13% 0.911% 22 35.568 3319 3325 3344 rBV 195395 622555 4.23% 0.630% 23 36.715 3442 3450 3465 rBV2 111771 415732 2.83% 0.420% 24 37.119 3486 3494 3521 rBV2 1840835 5935431 40.36% 6.002% 25 38.010 3584 3591 3605 rBV2 50461 221447 1.51% 0.224%

Sum of corrected areas: 98896226

NYC-WTC_000018448

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NYC-WTC_000018448Source: NYC Law Department, mirrored locally

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