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GC/MS calibration data for sample 30647, Dec 2001

Machine-extracted title · confidence 100%

Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.

NYC-WTC_000018546–000018575

Folder label: “GCMS X 12/18/01 A 12/30/01

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NYC 9/11 Public Portal Document LSC Area Percent Report

•Data File : C:\HPCHEM\1\DATA\DEC2701\30706.D Vial: 54 Acq On : 30 Dec 2001 12:10 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/18 A Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.613 276 280 311 rBV 600085 1640614 14.10% 2.406% 2 11.129 657 663 671 rBV 208419 498088 4.28% 0.730% 3 11.670 717 722 744 rBV 3234158 8300470 71.34% 12.171% 4 14.305 998 1009 1018 rBV 836865 1794233 15.42% 2.631% 5 15.278 1109 1115 1134 rBV 4469171 10432345 89.66% 15.297%

6 17.454 1344 1352 1362 rBV 1290411 2852289 24.51% 4.182% 7 18.161 1424 1429 1436 rBV 62564 135608 1.17% 0.199% 8 20.272 1653 1659 1667 rBV 844718 1867946 16.05% 2.739% 9 20.566 1684 1691 1708 rBV 4583818 11160887 95.92% 16.365% 10 21.034 1737 1742 1755 rBV 171119 611783 5.26% 0.897%'

11 22.788 1927 1933 1942 rVB 509829 1102083 9.47% 1.616% 12 24.982 2163 2172 2207 rBV2 4077866 11635614 100.00% 17.061% 13 26.891 2372 2380 2386 rBV 211884 452689 3.89% 0.664% 14 27.011 2388 2393 2406 rVB 67926 191035 1.64% 0.280% 15 28.654 2567 2572 2577 rBV 152848 331102 2.85% 0.485%

16 30.059 2720 2725 2735 rBV 466257 1084489 9.32% 1.590% 17 30.251 2739 2746 2754 rW 121162 282378 2.43% 0.414% 18 31.720 2901 2906 2915 rVB 93165 218151 1.87% 0.320% 19 33.024 3038 3048 3074 rBV2 2841476 8088712 69.52% 11.860% 20 33.299 3074 3078 3093 rVB 46938 135965 1.17% 0.199%

21 34.373 3190 3195 3204 rVB2 42758 117779 1.01% 0.173% 22 37.118 3486 3494 3521 rBV2 1590464 5265627 45.25% 7.721%

Sum of corrected areas: 68199887

30706.D GCMS1126.M Fri Feb 01 11:07:35 2 002

NYC-WTC_000018559

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NYC-WTC_000018559Source: NYC Law Department, mirrored locally

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