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Document / 344 pages

DEP GCMS data table, Jan-Feb 2002

Machine-extracted title · confidence 90%

Large multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

NYC-WTC_000004149–000004492

Folder label: “GCMS X 12/18/01, 2/8/02 A 2/10/02, 1/10/02, 1/14/02

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Scanned page image, NYC-WTC_000004308
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NYC 9/11 Public Portal Document LSC Area Percent Report

. Data File : C:\HPCHEM\1\DATA\DEC2 701\30709.D Vial: 47 Acq On : 30 Dec 2001 4:24 am Operator: 209 GALOS Sample : GC/MS SCAN 12/18 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.615 276 280 312 rVB 427192 1313171 9.62% 1.612% 2 11.673 717 722 752 rBV 3618330 9598800 70.32% 11.783% 3 14.308 1000 1009 1016 rBV 349814 742071 5.44% 0.911% 4 15.281 1109 1115 1134 rBV 5010412 11823359 86.62% 14.513% 5 17.447 1342 1351 1358 rBV 1501430 3305742 24.22% 4.058%

6 18.154 1423 1428 1435 rBV 147128 287524 2.11% 0.353% 7 20.275 1651 1659 1668 rBV 1508999 3231155 23.67% 3.966% 8 20.559 1683 1690 1706 rBV 5523685 12794648 93.73% 15.706% 9 21.018 1733 1740 1762 rBV 403676 1254933 9.19% 1.540% 10 22.790 1926 1933 1943 rBV 1071203 2291904 16.79% 2.813%

11 24.984 2162 2172 2186 rBV3 4897948 13650212 100.00% 16.756% 12 26.885 2373 2379 2387 rBV 552205 1192197 8.73% 1.463% 13 28.647 2565 2571 2581 rBV 415946 944396 6.92% 1.159% 14 30.061 2717 2725 2734 rBV 536638 1120073 8.21% 1.375% 15 30.245 2740 2745 2758 rVB 371902 858264 6.29% 1.054%

16 31.713 2898 2905 2918 rBV 325133 764444 5.60% 0.938% 17 33.026 3040 3048 3053 rBV2 3576138 8847685 64.82% 10.861% 18 34.376 3188 3195 3208 rBV 187668 551810 4.04% 0.677% 19 35.569 3319 3325 3336 rBV 120798 361227 2.65% 0.443% 20 36.717 3442 3450 3460 rBV2 65496 218333 1.60% 0.268%

21 37.121 3486 3494 3522 rBV 2020076 6173017 45.22% 7.578% 22 38.020 3583 3592 3603 rBV 33141 139789 1.02% 0.172%

Sum of corrected areas: 81464754

30709.D GCMS1126.M Mon Jan 28 11:32:23 2002

NYC-WTC_000004308

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NYC-WTC_000004308Source: NYC Law Department, mirrored locally

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