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GCMS analysis results for sample AD29523, Jan 2002

Machine-extracted title · confidence 100%

GCMS analysis report for sample AD29523 listing unknown compounds and surrogate recovery data from January 28, 2002.

NYC-WTC_000036798–000036814

Folder label: “GCMS X 12/7/01 A 1/2/02”

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NYC 9/11 Public Portal Document

LSC Area Percent Report

• Data File : C:\HPCHEM\1\DATA\DEC2701\29523.D Vial: 37 Acq On : 29 Dec 2001 12:10 am Operator: 209 GALOS Sample : GC/MS SCAN 12/7 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.612 276 280 298 rBV 474021 1343284 10.38% 1.896% 2 11.128 658 663 671 rBV 145510 351051 2.71% 0.495% 3 11.678 718 723 754 rBV 3783854 9891934 76.44% 13.960% 4 14.304 1003 1009 1020 rVB 428963 931832 7.20% 1.315% 5 15.286 1109 1116 1134 rBV 5080284 12163237 93'. 99% 17.165%

6 17.453 1345 1352 1361 rBV 677538 1409539 10.89% 1.989% 7 20.271 1653 1659 1669 rBV 449099 976746 7.55% 1.378% 8 20.565 1684 1691 1716 rBV 5500471 12940609 100.00% 18.262% 9 21.042 1738 1743 1757 rBV 75517 339768 2.63% 0.479% 10 22.787 1928 1933 1942 rBV 293882 607357 4.69% 0.857%

11 24.990 2162 2173 2186 rBV2 4838147 12692321 98.08% 17.912% 12 26.890 2374 2380 2387 rBV 131656 281102 2.17% 0.397% 13 28.653 2563.2572 2579 rBV 98679 215847 1.67% 0.305% 14 30.057 2720 2725 2734 rBV 487782 1102724 8.52% 1.556% 15 30.250 2740 2746 2754 rVB 81878 184923 1.43% 0.261%

16 31.719 2899 2906 2915 rBV 60414 156331 1.21% 0.221% 17 33.032 3041 3049 3074 rBV2 3458793 9126242 70.52% 12.879% 18 37.126 3486 3495 3521 rBV 1948223 6145744 47.49% 8.673%

Sum of corrected areas: 70860591

29523 .D GCMS1126.M Tue Jan 08 12:09:09 2002

NYC-WTC_000036803

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NYC-WTC_000036803Source: NYC Law Department, mirrored locally

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Large multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

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