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GCMS analysis comments, sample AD28802, Dec 2001

Machine-extracted title · confidence 95%

GCMS scan results for sample AD28802 dated December 16, 2001, detecting bis(2-Ethylhexyl)phthalate and other compounds.

NYC-WTC_000035460–000035472

Folder label: “GCMS X 11/27/01 A 12/7/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

- Data File C:\HPCHEM\1\DATA\DEC0601\28802 .D Vial 29 Acq On 7 Dec 2001 3:00 am Operator 209 GALOS Sample 11/27 gc/ms scan Inst GC/MS 209 Mise Multiplr 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge 100 prefer < Baseline drop else tangent Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 6.327 137 14 0 143 rBV 63864 119442 1.44% 0.246% 2 6.438 149 152 160 rBV2 111778 250869 3 ; 03% 0.516% 3 6.658 172 176 194 rVB 129679 328551 3.96% 0.676% 4 7.686 285 288 3 08 rW 590058 1533118 18.50% 3.154% 5 10.137 549 555 565 rBV 32810 85462 1.03% 0.176%

6 10.339 573 577 585 rBV 38047 96680 1.17% 0.199% 7 10.660 607 612 622 rVB 42353 103542 1.25% 0.213% 8 11.670 717 722 741 rBV 2404350 5845952 70.55% 12.026% 9 14.305 1004 1009 1015 rVB 51188 98875 1.19% 0.203% 10 15.278 1109 1115 1129 rBV 3595588 7647551 92.29% 15.732%

11 20.557 1683 1690 1713 rBV 3710827 8286542 100.00% 17.047% 12 24.973 2165 2171 2183 rBV2 3490706 7880702 95.10% 16.212% 13 25.119 2183 2187 2199 rVB 30386 97689 1.18% 0.201% 14 30.049 2718 2724 2731 rBV 527617 1049421 12.66% 2.159% 15 33.005 3039 3046 3066 rBV2 2509508 6052200 73.04% 12.451%

16 33.290 3072 3077 3085 rBV 50066 121559 1.47% 0.250% 17 35.567 3319 3325 3345 rBV 1547342 3998367 48.25% 8.225% 18 37.100 3484 3492 3512 rBV2 1756703 5013410 60.50% 10.314%

Sum of corrected areas: 48609932

28802.D GCMS1126.M Wed Dec 12 11:34:30 2001

NYC-WTC_000035465

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NYC-WTC_000035465Source: NYC Law Department, mirrored locally

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