GCMS comments for sample AD28901, Dec 17 2001

NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\HPCHEM\1\DATA\DEC0 601\28901.D Vial: 38 Acq On 7 Dec 2001 11:48 am Operator: 209 GALOS Sample 11/28 gc/ms scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.609 275 279 290 rBV 72542 183797 2.28% 0.354% 2 11.676 716 722 741 rBV 2296692 5717334 71.00% 11.022% 3 15.275 1108 1114 1132 rBV 3470623 7585261 94.20% 14.623% 4 20.553 1683 1689 1714 rBV 3563994 8052406 100.00% 15.524% 5 24.978 2164 2171 2183 rBV2 3405094 7642489 94.91% 14.734%

6 30.055 2718 2724 2732 rBV 428097 876327 10.88% 1.689% 7 33.011 3039 3046 3069 rBV2 2571394 6125249 76.07% 11.809% 8 34.370 3187 3194 3206 rBV 132649 410952 5.10% 0.792% 9 35.563 3318 3324 3346 rBV2 389973 1461694 18.15% 2.818% 10 36.711 3441 3449 3473 rBV 352863 1537009 19.09% 2.963%

11 37.106 3484 3492 3514 rBV2 1828092 5220786 64.84% 10.065% 12 38.014 3581 3591 3610 rBV 352007 1889278 23.46% 3.642% 13 39.584 3751 3762 3789 rBV3 281769 1925203 23.91% 3.712% 14 41.521 3960 3973 3994 rBV3 190537 1518331 18.86% 2.927% 15 43.945 4221 4237 4263 rBV2 113653 1092790 13.57% 2.107%

16 47.020 4554 4572 4598 .rBV5 58553 631972 7.85% 1.218%

Sum of corrected areas: 51870878

28901.D GCMS1126.M Tue Dec 11 16:07:54 2001

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