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GCMS comments for sample AD28899, Dec 17 2001

Machine-extracted title · confidence 90%

Laboratory notes identifying potential laboratory contamination by specific esters in sample AD28899.

NYC-WTC_000035717–000035726

Folder label: “GCMS X 11/28/01 A 12/7/01

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Scanned page image, NYC-WTC_000035722
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NYC 9/11 Public Portal Document

LSC Area Percent Report Data File C: \HPCHEM\ 1 \DATA\DEC0601\28899.D Vial: 7 Acq On 6 Dec 2001 7:11 pm Operator: 209 GALOS Sample 11/28 gc/ms scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.609 275 279 291 rBV 116177 333949 4.23% 0.781% 2 7.747 291 294 312 rVB2 26962 112769 1.43% 0.264% 3 11.676 716 722 741 rBV 2092027 5727815 72.64% 13.402% 4 15.275 1108 1114 1132 rBV 3436394 7479979 94.86% 17.502% 5 20.553 1683 1689 1705 rBV 3683726 7885677 100.00% 18.451%

6 24.978 2164 2171 2182 rBV2 3408395 7616972 96.59% 17.823% 7 25.116 2182 2186 2194 rVB 30889 87252 1.11% 0.204% 8 26.989 2384 2390 2396 rBV 44443 87332 1.11% 0.204% 9 30.055 2718 2724 2731 rBV 387438 820678 10.41% 1.920% 10 33.011 3039 3046 3060 rBV2 2707266 6433937 81.59% 15.054%

11 33.286 3071 3076 3086 rVB2 30334 82786 1.05% 0.194% 12 35.563 3319 3324 3337 rBV 97691 311682 3.95% 0.729% 13 37.105 3482 3492 3510 rBV2 1971047 5757088 73.01% 13.471%

Sum of corrected areas: 42737916

28899.D GCMS1126.M Tue Dec 11 16:05:57 2001

NYC-WTC_000035722

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NYC-WTC_000035722Source: NYC Law Department, mirrored locally

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