Laboratory GCMS analysis report for sample AD29229 conducted on December 28, 2001, including surrogate recovery data.
NYC-WTC_000036325–000036336Folder label: “GCMS X 12/4/01 A 12/10/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
LSC Area Percent Report
Data File C: \HPCHEM\1\DATA\DEC1201\29229.D Vial: 12 Acq On 12 Dec 2001 12:44 pm Operator: 209 GALOS Sample gc/ms scan 12/4 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP
If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5
Signal TIC
peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total
1 7.599 273 278 308 rBV 401530 1127355 16.40% 2.997% 2 11.336 681 685 690 rBV 268056 578754 8.42% 1.539% 3 11.409 690 693 713 rVB 275936 738053 10.73% 1.962% 4 11.666 713 721 745 rBV2 2021304 5901974 85.84% 15.692% 5 15.274 1108 1114 1133 rBV 2973954 6364788 92.58% 16.923%
6 20.553 1683 1689 1707 rBV 3155420 6875246 100.00% 18.280% 7 24.969 2164 2170 2182 rBV2 2764017 6392099 92.97% 16.995% 8 25.116 2183 2186 2194 rVB 25078 68783 1.00% 0.183% 9 26.988 2383 2390 2398 rBV 36153 83214 1.21% 0.221% 10 30.045 2718 2723 2733 rBV 426885 912149 13.27% 2.425%
11 33.001 3036 3045 3066 rBV2 1959278 4810299 69.97% 12.790% 12 35.563 3319 3324 3334 rBV 52163 150628 2.19% 0.400% 13 37.096 3483 3491 3509 rBV2 1270326 3607859 52.48% 9.593%
Sum of corrected areas: 37611201
29229.D GCMS1126.M Fri Dec 28 15:27:39 2001
NYC-WTC_000036330
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NYC-WTC_000036300
Laboratory analysis report for sample AD29456 conducted on December 28, 2001, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036278
Laboratory analysis report for sample AD29296 conducted on December 28, 2001, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036092
Laboratory report noting GCMS scan results for sample AD29234 with one compound recovery outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035865
Lab notes for sample AD29134 indicate detection of di-n-butylphthalate and one LCS compound outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036220
Blank sample results showing non-detect levels for target compounds during December 2001 laboratory testing.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036255
Laboratory analysis report for sample AD29294 conducted on December 28, 2001, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036289
Laboratory analysis report for sample AD29455 conducted on December 28, 2001, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035853
Lab notes for sample AD29139 indicate detection of di-n-butylphthalate and one LCS compound outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036267
Laboratory analysis report for sample AD29295 conducted on December 28, 2001, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036151
Laboratory report noting GCMS scan results for sample AD29231 with phthalates detected and low recovery requiring re-analysis.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035831
Lab notes for sample AD29141 indicate detection of bis(2-Ethylhexyl)phthalate and one LCS compound outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036243
Laboratory analysis report for sample AD29235 conducted on December 28, 2001, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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NYC-WTC_000036199
Department of Environmental Protection record logging GCMS X samples from November to December 2001.
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NYC-WTC_000036200
Laboratory methodology table documenting sample extraction parameters, surrogate recovery rates, and quality control data for mass spectrometry analysis.
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NYC-WTC_000036201
Laboratory record documenting the extraction method parameters for sample AD29229 analyzed in December 2001.
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NYC-WTC_000036205
Calibration data for volatile organic compounds including nitrosamines and chlorinated solvents from December 2001.
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NYC-WTC_000036210
Reference analysis results for target analytes used to verify GCMS instrument performance in December 2001.
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