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GCMS analysis comments, sample AD28964, Dec 2001

Machine-extracted title · confidence 90%

Lab report noting bis(2-Ethylhexyl)phthalate detection, recovery issues, and low pH.

NYC-WTC_000035640–000035650

Folder label: “GCMS X 11/29/01 A 12/7/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\HPCHEM\l\DATA\DEC0701\28964.D Vial: 10 Acq On 7 Dec 2001 11:43 pm Operator: 209 GALOS Sample 11/29 gc/ms scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop- else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.608 275 279 312 rVB 276988 834933 12.10% 2.386% 2 11.345 683 686 692 rBV 53207 132209 1.92% 0.378% 3 11.427 692 695 716 rVB 60523 185233 2.69% 0.529% 4 11.675 716 722 740 rBV 1875590 4960912 71.92% 14.177% 5 15.274 1109 1114 1133 rBV 2930976 6307547 91.44% 18.026%

6 20.553 1683 1689 1705 rBV 3180081 6898070 100.00% 19.714% 7 24.978 2164 2171 2183 rBV2 2984230 6460679 93.66% 18.464% 8 25.115 2183 2186 2196 rVB 29127 81748 1.19% 0.234% 9 30.054 2718 2724 2731 rVB 371118 759540 11.01% 2.171% 10 33.010 3039 3046 3062 rBV2 2008764 4725054 68.50% 13.503%

11 33.295 3071 3077 3088 rVB 54492 142536 2.07% 0.407% 12 37.105 3484 3492 3517 rBV2 1220013 3503089 50.78% 10.011%

Sum of corrected areas: 34991550

28964.D GCMS1126.M Thu Dec 13 10:19:42 2001

NYC-WTC_000035645

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NYC-WTC_000035645Source: NYC Law Department, mirrored locally

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